ChemicalBook Product Catalog Chemical Reagents Organic reagents Sulfone, sulfoxide compound DI-N-BUTYL SULFONE

DI-N-BUTYL SULFONE

DI-N-BUTYL SULFONE Basic information
Product Name:DI-N-BUTYL SULFONE
Synonyms:1-(Butane-1-sulfonyl)-butane;1-(Butylsulfonyl)butane;1,1’-sulfonylbis-butan;1,1'-Sulphonylbisbutane;Butane,1,1-sulfonylbis-;Di-n-butyl sufone;BUTYL SULFONE;DI-N-BUTYL SULFONE
CAS:598-04-9
MF:C8H18O2S
MW:178.29
EINECS:209-914-6
Product Categories:Industrial/Fine Chemicals
Mol File:598-04-9.mol
DI-N-BUTYL SULFONE Structure
DI-N-BUTYL SULFONE Chemical Properties
Melting point 43-45 °C(lit.)
Boiling point 287-295 °C(lit.)
density 0.9885
refractive index 1.4433
Fp 290 °F
BRN 1722269
CAS DataBase Reference598-04-9(CAS DataBase Reference)
EPA Substance Registry SystemButane, 1,1'-sulfonylbis- (598-04-9)
Safety Information
WGK Germany 3
TSCA Yes
MSDS Information
ProviderLanguage
SigmaAldrich English
ALFA English
DI-N-BUTYL SULFONE Usage And Synthesis
Chemical PropertiesLIGHT BEIGE ADHERING CRYSTALS
Synthesis Reference(s)The Journal of Organic Chemistry, 47, p. 2790, 1982 DOI: 10.1021/jo00135a024
Synthesis, p. 299, 1978 DOI: 10.1055/s-1978-24730
Tetrahedron Letters, 22, p. 1655, 1981 DOI: 10.1016/S0040-4039(01)90402-2
Purification MethodsPurify it by zone melting. It crystallises from pet ether (m 44-44.5o), CHCl3 (m 44o), and EtOH (m 45o). [Beilstein 1 H 371, 1 II 400, 1 III 1524, 1 IV 1561.]
DI-N-BUTYL SULFONE Preparation Products And Raw materials
Raw materials1-Butanesulfonic acid-->DI-N-BUTYL SULFOXIDE-->Butyl disulfide-->Butyraldehyde
Preparation ProductsDibutyl sulfide
DI-N-AMYL SULFOXIDE DODECYL SULFONE 3-(CYCLOHEXYLSULFONYL)-4-METHYLTETRAHYDRO-2H-PYRAN-4-OL AKOS 90823 3-[7a-Methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-2,2-dioxo-2,3,4,5,6,7-hexahydro-1H-2l6-benzo[c]thiophen-5-ol AKOS 90802 AKOS BBS-00004948 BOC-L-BUTHIONINESULFOXIMINE DI-N-HEXYL SULFONE tert-Butyl-dimethyl-{3-[7a-methyl-1-(1,4,5-trimethyl-hex-2-enyl)-octahydro-inden-4-ylidenemethyl]-2,2-dioxo-2,3,4,5,6,7-hexahydro-1H-2l6-benzo[c]thiophen-5-yloxy}-silane AKOS 90072 DIISOAMYL SULFONE BIS(ETHYLHEXYL)SULPHONE DI-N-DECYL SULPHONE AKOS 90406 DI-N-OCTYL SULFONE N-NONYLSULPHONE 2-{4-[6-(tert-Butyl-dimethyl-silanyloxy)-2,2-dioxo-2,3,4,5,6,7-hexahydro-1H-2l6-benzo[c]thiophen-1-ylmethylene]-7a-methyl-octahydro-inden-1-yl}-propan-1-ol
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