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| | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) Basic information |
| Product Name: | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) | | Synonyms: | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol);5,5'-(1-Methylethylidene)bis(2-hydroxy-1,3-benzenedimethanol);1,3-Benzenedimethanol, 5,5'-(1-methylethylidene)bis(2-hydroxy-;Einecs 223-553-1;(propane-2,2-diylbis(2-hydroxybenzene-5,3,1-triyl))tetramethanol;2,2-bis[4-hydroxy-3,5-di(hydroxymethyl)phenyl]propane;4-[2-[4-Hydroxy-3,5-Bis(Hydroxymethyl)Phenyl]Propan-2-Yl]-2,6-Bis(Hydroxymethyl)Phenol;948/2,2-bis[4-Hydroxy-3,5-di(hydroxymethyl)phenyl]propane | | CAS: | 3957-22-0 | | MF: | C19H24O6 | | MW: | 348.39 | | EINECS: | 223-553-1 | | Product Categories: | | | Mol File: | 3957-22-0.mol |  |
| | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) Chemical Properties |
| | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) Usage And Synthesis |
| Uses | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process. | | Synthesis | Preparation Example 3. 2,2-bis[4-trimethylsilyloxy-3,5-bis(trimethylsilyloxymethyl)-phenyl]propane (monomer K). a) 2,2-bis[4-hydroxy-3,5-di(hydroxymethyl)phenyl)]propane. 114.4 of bisphenol A (2,2-bis[4-hydroxyphenyl)]propane) were initially charged in a mixture of 450 g of water and 50 g of NaOH. While cooling (Tmax=25°C), 350 g of 30% formaldehyde solution were added dropwise. After continued reaction at room temperature for 1 h, a clear solution was obtained. The mixture was neutralized by adding solid CO2. The resulting solution was saturated with sodium chloride and extracted 3 times with butanol. The extracts were concentrated on a rotary evaporator at 50°C down to 5 mbar. The product was used in the next step without further purification. colorless oil. 1H-NMR 400 MHz, CDCl3, 25°C, TMS δ [ppm] = 7.03 (s, 4 H, Aromat); 5.00 (s, 6 H, -OH (breit)); 4.63 (s, 8H, -CH2-); 1.60 (s, 6 H, C-CH3). |
| | 5,5'-isopropylidenebis(m-xylene-2,alpha,alpha'-triol) Preparation Products And Raw materials |
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