Diethylamine hydrochloride

Diethylamine hydrochloride Basic information

Product Name:	Diethylamine hydrochloride
Synonyms:	Diethyl-ammonium;Ethanamine,N-ethyl-,hydrochloride;n-ethylethanaminehydrochloride;n-ethyl-ethanaminhydrochloride;METHYLENE BLUE STAIN SOLUTION, LOEFFLER'S;METHYLENE BLUE WATER AND ALCOHOL SOLUBLE;METHYLENE BLUE ZF;METHYLENE BLUE, ZINC-FREE
CAS:	660-68-4
MF:	C4H12ClN
MW:	109.6
EINECS:	211-541-9
Product Categories:	Amine Salts;Nitrogen Compounds;Organic Building Blocks;Pharmaceutical Intermediates;660-68-4
Mol File:	660-68-4.mol

Diethylamine hydrochloride Chemical Properties

Melting point	227-230 °C(lit.)
Boiling point	320-330 °C
density	1.0 g/mL at 20 °C
vapor pressure	<0.00001 hPa (20 °C)
refractive index	1.5320 (estimate)
Fp	320-330°C
storage temp.	Store below +30°C.
solubility	H2O: soluble50mg/mL, clear, colorless
form	Liquid
Specific Gravity	1.0475 (21℃)
color	White to off-white
PH	4.5-6.5 (10g/l, H2O, 20℃)
Water Solubility	soluble
Sensitive	Hygroscopic
Merck	14,3111
BRN	3590084
LogP	-1.3 at 20℃
CAS DataBase Reference	660-68-4(CAS DataBase Reference)
EPA Substance Registry System	Diethylamine hydrochloride (660-68-4)

Safety Information

Hazard Codes	Xn,Xi
Risk Statements	10-36/37/38
Safety Statements	26-39-7-24/25-36
RIDADR	UN 1993 3/PG 3
WGK Germany	3
RTECS	SP5740000
F	21
TSCA	Yes
HS Code	29211200
Toxicity	LD50 orally in Rabbit: 9900 mg/kg

MSDS Information

Provider	Language
Diethylamine hydrochloride	English
SigmaAldrich	English
ACROS	English
ALFA	English

Diethylamine hydrochloride Usage And Synthesis

Chemical Properties	white to off-white crystals or crystalline powder
Uses	Diethylamine hydrochloride acts as a precursor of atrazine and lysergic acid diethylamide. It is also used as a reactant in the production of dyes and pharmaceutical compounds such as ranitidine. Further, it is used in Mannich reaction with paraformaldehyde. In addition to this, it is employed in the synthesis of diethylaminoethyl (DEAE) cottons by reacting with cotton cellulose in the presence of sodium hydroxide.
Flammability and Explosibility	Notclassified
Purification Methods	Crystallise salt from absolute EtOH. Also crystallise it from dichloroethane/MeOH. Hygroscopic. [Beilstein 4 III 113.]

Diethylamine hydrochloride Preparation Products And Raw materials

Raw materials	Diethylamine-->Phosphinous amide, P,P-bis(3,5-dimethylphenyl)-N,N-diethyl--->BIS(3,5-DIMETHYLPHENYL)CHLOROPHOSPHINE-->tert-butyl 4-phenylpiperidine-1-carboxylate-->4-Phenylpiperidine
Preparation Products	N-(Carboxymethyl)-N-(phosphonomethyl)-glycine-->N,N-Diethyldecanamide-->1-DIETHYLAMINO-3-BUTANONE-->1,1-DIETHYLUREA-->N,N-DIETHYLCYCLOHEXYLAMINE-->Diethyl (trichloromethyl)phosphonate-->Oxolamine-->BIS(DIETHYLAMINO)CHLOROPHOSPHINE

2-Aminoethylmethylsulfone hydrochloride N-Chloroethyl-N-ethylaniline N,N'-OCTAMETHYLENEBIS(DICHLOROACETAMIDE) CI 52015 CI-52015 Topotecan hydrochloride CI NO 52015,CI 52015 N-[(2,6-DICHLORO-4-PYRIDYL)METHYL!-N,N-DIETHYLAMINE HYDROCHLORIDE, TECH (6-BROMOHEXYL) DIETHYLAMINE HYDROCHLORIDE 2-chloro-N-methyl-diethylamine, hydrochloride N-(2-AMINO-4-CHLOROPHENYL)-N,N-DIETHYLAMINE HYDROCHLORIDE (2-Mercaptoethyl)diethylamine·hydrochloride CI 52015 DIETHYLPROPION CHLOROACETYL-L-TYROSINE Cysteamine hydrochloride 2-[[(2-ethylphenyl)(2-hydroxyethyl)amino]methyl]-3,3-difluoro-Propanenitrile N-[(2,6-DICHLORO-4-PYRIDYL)METHYL]-N,N-DIETHYLAMINE HYDROCHLORIDE

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