Kryptofix 222

Kryptofix 222 Basic information

Product Name:	Kryptofix 222
Synonyms:	2,2,2-CRYPT;2,2,2-CRYPTAND;2,2,2-CRYPTATE;4,7,13,16,21,24-HEXAOXA-1,10-DIAZABICYCLO[8.8.8]HEXACOSANE;KRYPTAND 222;KRYPTOFIX 222;KRYPTOFIX(R) 222;CRYPTOFIX 222
CAS:	23978-09-8
MF:	C18H36N2O6
MW:	376.49
EINECS:	245-962-4
Product Categories:	FDG Chemicals;Azacrown Ethers;Crown Ethers;Functional Materials;Macrocycles for Host-Guest Chemistry;Crown EthersStable Isotopes;Chelation/Complexation Compounds;PET;Synthetic Reagents
Mol File:	23978-09-8.mol

Kryptofix 222 Chemical Properties

Melting point	68-71 °C(lit.)
Boiling point	505.03°C (rough estimate)
density	1.1888 (rough estimate)
refractive index	1.5700 (estimate)
storage temp.	Store at +2°C to +8°C.
solubility	Chloroform (Slightly), Methanol (Slightly, Heated)
form	Solid
pka	7.21±0.20(Predicted)
color	White to Off-White
Water Solubility	soluble
BRN	620282
InChIKey	AUFVJZSDSXXFOI-UHFFFAOYSA-N
CAS DataBase Reference	23978-09-8(CAS DataBase Reference)
NIST Chemistry Reference	4,7,13,16,21,24-Hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane(23978-09-8)

Safety Information

Hazard Codes	Xi,Xn
Risk Statements	36/37/38-22
Safety Statements	26-36-36/37/39
WGK Germany	3
RTECS	MP4750000
HS Code	2934 99 90
Toxicity	LD50 orally in Rabbit: > 300 - 2000 mg/kg

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English

Kryptofix 222 Usage And Synthesis

Chemical Properties	Colourless crystals
Uses	2,2,2-Crypt is used in the synthesis of hybrid metal-organic salts. It is also an impurity in the preparation of Fludeoxyglucose (D232570), a D-Glucose (G595000) derivative used in the synthesis of sugar nucleotides and oligosaccharides.

Kryptofix 222 Preparation Products And Raw materials

Raw materials

Tetrahydrofuran-->Dichloromethane-->Sodium-->Sodium carbonate-->Potassium hydroxide-->Triethylamine-->Ammonium hydroxide-->Ammonia-->Lithium Aluminum Hydride-->Acetonitrile-->1,4-Dioxane-->Sodium azide-->Tosyl chloride-->Methanesulfonyl chloride-->Triethylene glycol-->ALUMINUM OXIDE

N-(2-METHOXYETHYL)ETHYLAMINE Kryptofix 222 N-(2-METHOXYETHYL)METHYLAMINE N-Methyldiethanolamine N-Methyl-bis(2-methoxyethyl)amine 2-[2-(Dimethylamino)ethoxy]ethanol Diethylaminoethanol BIS(2-METHOXYETHYL)AMINE POLY(METHYLSILSESQUIOXANE) 6-Ethyl-3-oxa-6-azaoctanol 1,8-Diamino-3,6-dioxaoctane 2-(2-Aminoethoxy)ethanol BIS(2-ETHOXYETHYL)AMINE 2-Ethoxyethylamine 1,8-BIS(METHYLAMINO)-3,6-DIOXAOCTANE, 98 N,N-Dimethyl-2-methoxyethylamine 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE Triethanolamine

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