emylcamate

emylcamate Basic information

Product Name:	emylcamate
Synonyms:	3-methylpentan-3-yl carbamate;JD 91;KABI-925;MK-250;Nuncital;Statran;Striatran;carbamic acid (1-ethyl-1-methyl-propyl) ester
CAS:	78-28-4
MF:	C7H15NO2
MW:	145.2
EINECS:	2011014
Product Categories:
Mol File:	78-28-4.mol

emylcamate Chemical Properties

Melting point	56-58.5°
Boiling point	bp1.0 35°; bp0.7 24°
density	0.9441 (estimate)
refractive index	1.4206 (estimate)
pka	13.54±0.50(Predicted)
CAS DataBase Reference	78-28-4

Safety Information

Toxicity

LD50 oral in mouse: 760mg/kg

MSDS Information

emylcamate Usage And Synthesis

Originator	Striatin,MSD,US,1960
Uses	Emylcamate is used in combination with compounds that influence brain function and or psychological state to treat herpes virus infection and outbreaks.
Definition	ChEBI: Emylcamate is a carbamate ester.
Manufacturing Process	30.5 g of 3-methyl-3-pentanol, 8.1 g of potassium cyanate and 16.3 g of trichloroacetic acid are heated while stirring at 45°C to 50°C for 24 hours, neutralized by successive addition of anhydrous sodium carbonate. The precipitate is removed from the reaction mixture. Unreacted 3-methyl-3- pentanol is distilled off and the residue is added to a small volume of distilled water. After precipitation and filtration the resulting 3-methyl-3-pentanol carbamate is dried and recrystallized from petroleum ether. MP 54°C to 55°C.
Therapeutic Function	Tranquilizer
Purification Methods	Crystallise the carbamate from 30% aqueous EtOH. [Beilstein 1 IV 1773.]

emylcamate Preparation Products And Raw materials

Raw materials

Trichloroacetic acid-->Sodium carbonate-->3-Methyl-3-pentanol-->Potassium cyanate

1-Pentyn-3-ol,3-ethyl-,carbamate(9CI) 1-ETHYL-8,9-DIMETHOXY-1,10B-DIMETHYL-1,5,6,10B-TETRAHYDRO[1,3]OXAZOLO[4,3-A]ISOQUINOLIN-3-ONE emylcamate CBI-BB ZERO/001941 SPECS AG-205/37268014 3-[2-(3,4-DIMETHOXYPHENYL)ETHYL]-4-HYDROXY-4,5-DIMETHYL-5-(4-METHYL-3-PENTENYL)-1,3-OXAZOLIDIN-2-ONE ETHINAMATE SPECS AG-205/37153028 4-HYDROXY-4-METHYL-3-(2-PYRIDYLMETHYL)-1-OXA-3-AZASPIRO[4.5]DECAN-2-ONE 3-ALLYL-4-HYDROXY-4,5-DIMETHYL-5-(4-METHYL-3-PENTENYL)-1,3-OXAZOLIDIN-2-ONE CBI-BB ZERO/001962 1,3-dimethyl-7-[2-oxo-2-(2-oxo-8-phenethyl-1-oxa-3,8-diazaspiro[4.5]dec-3-yl)ethyl]purine-2,6-dione CBI-BB ZERO/001957 fenspiride vinzolidine 4,4,6A,6B-TETRAMETHYLHEXAHYDRO-3H-1-OXA-2A,3-DIAZACYCLOPENTA[CD]PENTALEN-2-ONE 4,4,6A,6B-TETRAMETHYL-3-PHENYLHEXAHYDRO-3H-1-OXA-2A,3-DIAZACYCLOPENTA[CD]PENTALEN-2-ONE 1-MENTHHYDRAZIDE

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