ChemicalBook Product Catalog Chemical Reagents Organic reagents Olefin (cyclic and acyclic) 1H,1H,2H-Perfluoro-1-decene

1H,1H,2H-Perfluoro-1-decene

1H,1H,2H-Perfluoro-1-decene Basic information
Product Name:1H,1H,2H-Perfluoro-1-decene
Synonyms:3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluoro-1-decene,99%;(Perfluoroct-1-yl)ethylene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluorodec-1-ene;1H,1H,2H-Heptadecafluorodec-1-ene 97%;1H,1H,2H-Perfluoro-1-decene 99%;1,1,2-Trihydroperfluoro-1-decene;1H,1H,2H-PERFLUORODEC-1-ENE;1H,1H,2H-PERFLUORO-1-DECENE;1H,1H,2H-HEPTADECAFLUORO-1-DECENE
CAS:21652-58-4
MF:C10H3F17
MW:446.1
EINECS:244-503-5
Product Categories:Fluorous Compounds;Synthetic Organic Chemistry;Fluorous Chemistry
Mol File:21652-58-4.mol
1H,1H,2H-Perfluoro-1-decene Structure
1H,1H,2H-Perfluoro-1-decene Chemical Properties
Boiling point 146-147 °C
density 1.677 g/mL at 25 °C (lit.)
refractive index n20/D 1.301(lit.)
Fp >230 °F
storage temp. Refrigerator
solubility Chloroform (Sparingly), Methanol (Slightly)
form Oil
color Colourless
Specific Gravity1.677
Water Solubility Insoluble in water.
BRN 2066558
InChIKeyNKAMGQZDVMQEJL-UHFFFAOYSA-N
CAS DataBase Reference21652-58-4(CAS DataBase Reference)
NIST Chemistry Reference1h,1h,2h-Perfluoro-1-decene(21652-58-4)
EPA Substance Registry SystemPerfluorooctyl Ethylene (21652-58-4)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
RIDADR 1993
WGK Germany 3
Hazard Note Harmful
TSCA T
HazardClass 3.2
PackingGroup III
HS Code 29033990
MSDS Information
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1H,1H,2H-Perfluoro-1-decene English
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1H,1H,2H-Perfluoro-1-decene Usage And Synthesis
Chemical Propertiesclear colorless liquid
Uses1H,1H,2H-Perfluoro-1-decene is useful in the chemical process of making an electrolyte-phobic surface for next generation nanostructured battery electrodes.
Synthesis 98% sodium hydroxide 108.535 mmol and methanol 38.74g were introduced into a 200mL eggplant flask which was equipped with a Dimroth condenser, the mixture was stirred at 50 °C until sodium hydroxide was dissolved. Sodium hydroxide amount to 1 liter of methanol in this case was 2.17 mol. After the sodium hydroxide had dissolved 1H, 1H, 2H, 2H-1-iodoperfluorodecane 104.996mmol was charged and further stirred for 2 hours at 50 °C. Heating and stirring were stopped, the obtained two-layer solution which became slightly pale brown turbid was separated after standing, and 45.81g lower layer was collected as 1H,1H,2H-perfluorodecene. As a result of analysis by gas chromatography, purity was 98.59%. The weight of the separated methanol layer was 56.10g.
synthesis of 1H,1H,2H-Perfluoro-1-decene
1H,1H,2H-Perfluoro-1-decene Preparation Products And Raw materials
Preparation Products1H,1H,2H,2H-PERFLUORODECYLMETHYLDICHLOROSILANE-->1H,1H,2H,2H-Perfluorodecyltrichlorosilane-->2-Bromo-1H,1H-perfluorodec-1-en-->1H,1H,2H,2H-Perfluorodecyltriethoxysilane
1H,1H,2H,2H-Perfluorohexyl iodide GALDEN (TM) HT70 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane Hexafluoropropylene oxide Perfluoroalkyl Ethylenes (Perfluorohexyl)ethylene Perfluoroalkylethyl acrylate Perfluoroalkyl alcohol 1-Iodoperfluoro-C6-12-alkanes 2-(Perfluoroalkyl)ethyl methacrylate 1H,1H,2H,3H-PERFLUOROUNDEC-2-EN-1-OL 11-(PERFLUORO-N-OCTYL)UNDEC-10-EN-1-OL 1H,1H,2H-Perfluoro-1-decene Perfluorotriethylamine Ethyleneamines 2-IODO-1H,1H,3H-PERFLUOROUNDEC-2-ENE-1-OL Perfluoro-1-decene 1H,1H,3H-2-IODOPERFLUOROUNDEC-2-EN-1-OL
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