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BORANE-N,N-DIETHYLANILINE COMPLEX

BORANE-N,N-DIETHYLANILINE COMPLEX Basic information
Product Name:BORANE-N,N-DIETHYLANILINE COMPLEX
Synonyms:BORANE-N,N-DIETHYLANILINE;BORANE-N,N-DIETHYLANILINE COMPLEX;n,n-diethylanilineborane,deanb;n-diethylbenzenamine)trihydro-((beta-4)-boro;(N,N-diethylaniline)trihydroboron;Borane-N,N-diethylaniline complex,97%;N, N diethylaniline borane complex;Borane-N,N-diethylaniline complex ,96%
CAS:13289-97-9
MF:C10H18BN
MW:163.07
EINECS:236-305-2
Product Categories:B (Classes of Boron Compounds);Boranes;Reduction;Synthetic Organic Chemistry;Synthetic Reagents
Mol File:13289-97-9.mol
BORANE-N,N-DIETHYLANILINE COMPLEX Structure
BORANE-N,N-DIETHYLANILINE COMPLEX Chemical Properties
Melting point −30-−27 °C(lit.)
density 0.917 g/mL at 25 °C(lit.)
refractive index 1.5245-1.5265
Fp 70 °F
storage temp. Refrigerator
form Liquid
color Clear colorless to yellow
Water Solubility MAY DECOMPOSE
InChIKeyYPWBYWNNJVSNPQ-UHFFFAOYSA-N
CAS DataBase Reference13289-97-9(CAS DataBase Reference)
EPA Substance Registry SystemBoron, (N,N-diethylbenzenamine)trihydro-, (T-4)- (13289-97-9)
Safety Information
Risk Statements 10-14-51/53-33-23/24/25-14/15
Safety Statements 16-33-36/37/39-43-9-61-45-28A-8
RIDADR UN 3398 4.3/PG 2
WGK Germany 3
HazardClass 3.1
PackingGroup II
HS Code 29299090
MSDS Information
ProviderLanguage
ACROS English
SigmaAldrich English
BORANE-N,N-DIETHYLANILINE COMPLEX Usage And Synthesis
Chemical Propertiesclear colorless to amber liquid
UsesReactant for:
  • Diastereoselective reduction of prochiral enone intermediates
  • Borylation of aryl halides
  • Reductions of ketones, acids, esters, amides, and nitriles
  • Investigations of borane source on enantioselectivity in enantiopure oxazaborolidine-catalyzed asymmetric borane reduction of ketones

Reactant for synthesis of:
  • Chromanol derivatives as CETP inhibitors for the treatment of cardiovascular disease
  • Allylic alcohols via enantioselective reductions
  • Pinacolboranes for one-pot synthesis of unsymmetrical biaryls
BORANE-N,N-DIETHYLANILINE COMPLEX Preparation Products And Raw materials
Raw materialsN,N-DIETHYLANILINE HYDROCHLORIDE-->Borane-tetrahydrofuran complex-->Diborane-->Sodium borohydride-->N,N-Diethylaniline-->Tributyltin Hydride-->Boron trichloride
Boronic acid, (2,3,6,7-tetrahydro-1H,5H-benzo[ij]quinolizin-9-yl)- (9CI) BORONIC ACID, B-[3-(1-PIPERIDINYL)PHENYL]- Boron 3-MALEIMIDOPHENYL BORONIC ACID 4-(1-PIPERIDINYL)PHENYLBORONIC ACID HCL 2-(MORPHOLINO)PHENYLBORONIC ACID 4-(PIPERIDINO)PHENYLBORONIC ACID 2,5-DIBUTOXY-4-(4-MORPHOLINYL)BENZENEDIAZONIUM TETRAFLUOROBORATE (4-PYRROLIDIN-1-YLPHENYL)BORONIC ACID 2-(1-PIPERIDINYL)PHENYLBORONIC ACID 3-(PYRROLIDINO)PHENYLBORONIC ACID 4-Morpholinophenylboronic acid 4-(DIETHYLAMINO)-2-ETHOXYBENZENEDIAZONIUM TETRAFLUOROBORATE 6-CHLORO-2-[2-(3-[(6-CHLORO-1-ETHYLBENZ[C,D,]INDOLE-2[1H]-YLIDENE)ETHYLIDENE]-2-PHENYL-1-CYCLOPENTEN-1-YL)ETHENYL]-1-ETHYLBENZ[C,D]INDOLIUM TETRAFLUOROBORATE 2,5-DIETHOXY-6-MORPHOLINO-BENZENE-DIAZONIUM-TETRAFLUOROBORATE 1-BUTYL-2-[2-[3-[(1-BUTYL-6-CHLORO-BENZ[CD]INDOL-2(1 H)-YLIDENE)ETHYLIDENE]-2-CHLORO-5-METHYL-1-CYCLOHEXEN-1-YL]ETHENYL]-6-CHLOROBENZ[CD]INDOLIUM TETRAFLUOROBORATE 1-BUTYL-2-[2-[3-[(1-BUTYL-6-CHLOROBENZ[CD]INDOL-2(1H)-YLIDENE)ETHYLIDENE]-2-CHLORO-1-CYCLOHEXEN-1-YL]ETHENYL]-6-CHLOROBENZ[CD]INDOLIUM TETRAFLUOROBORATE 4-DIAZO-N,N-DIETHYLANILINE FLUOROBORATE
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