ChemicalBook Product Catalog Organic Chemistry Carboxylic acids and derivatives Carboxylic acid halides CARBAZOLE-N-CARBONYL CHLORIDE

CARBAZOLE-N-CARBONYL CHLORIDE

CARBAZOLE-N-CARBONYL CHLORIDE Basic information
Product Name:CARBAZOLE-N-CARBONYL CHLORIDE
Synonyms:CARBAZOLE-N-CARBONYL CHLORIDE;CARBAZOLE-9-CARBONYL CHLORIDE;9-(CHLOROFORMYL)CARBAZOLE;N-(CHLOROCARBONYL)CARBAZOLE;CARBAZOLE-9-CARBONYL CHLORIDE, FOR FLUOR ESCENCE;9-(Chlorocarbonyl)carbazole;9-(Chloroformyl)-9H-carbazole;9H-Carbazole-9-carbonyl chloride
CAS:73500-82-0
MF:C13H8ClNO
MW:229.66
EINECS:
Product Categories:Functional Materials;Reagents for Conducting Polymer Research;Carbazoles;Carbazoles (for Conduting Polymer Research)
Mol File:73500-82-0.mol
CARBAZOLE-N-CARBONYL CHLORIDE Structure
CARBAZOLE-N-CARBONYL CHLORIDE Chemical Properties
Melting point 100-104 °C
Boiling point 407.5±28.0 °C(Predicted)
density 1.32±0.1 g/cm3(Predicted)
storage temp. 2-8°C
form powder to crystal
color White to Almost white
CAS DataBase Reference73500-82-0
Safety Information
Hazard Codes Xi
Risk Statements 36/38
Safety Statements 26-36
WGK Germany 3
F 10-21
HS Code 2928.00.5000
MSDS Information
ProviderLanguage
SigmaAldrich English
CARBAZOLE-N-CARBONYL CHLORIDE Usage And Synthesis
Purification MethodsRecrystallise the acid chloride from *C6H6. If it is not very pure (presence of OH or NH bands in the IR), dissolve it in pyridine, shake it with phosgene in toluene, evaporate and recrystallise the residue. Carry out this experiment in a good fume cupboard as COCl2 is very TOXIC, and store the product in the dark. It is moisture sensitive. The amide has m 246.5-247o, and the dimethylaminoethylamide hydrochloride has m 197-198o. [Weston et al. J Am Chem Soc 75 4006 1953, Beilstein 20 III/IV 3841.]
CARBAZOLE-N-CARBONYL CHLORIDE Preparation Products And Raw materials
N-ETHYL-6-BROMO-CARBAZOLE Deionized water CARBAZOLE-N-CARBONYL CHLORIDE N-METHYLCARBAZOLE Carbazole
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