1,6-Diisopropyl-3,8-dibromopyrene

1,6-Diisopropyl-3,8-dibromopyrene Basic information
Product Name:1,6-Diisopropyl-3,8-dibromopyrene
Synonyms:1,6-Diisopropyl-3,8-dibromopyrene;1,6-dibromo-3,8-diisopropylpyrene;Pyrene,1,6-dibromo -3,8-bis(1-methylethyl)-
CAS:869340-02-3
MF:C22H20Br2
MW:444.2
EINECS:
Product Categories:
Mol File:869340-02-3.mol
1,6-Diisopropyl-3,8-dibromopyrene Structure
1,6-Diisopropyl-3,8-dibromopyrene Chemical Properties
Boiling point 512.4±45.0 °C(Predicted)
density 1.508±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form powder to crystal
color White to Orange to Green
Safety Information
HS Code 2903.99.8001
MSDS Information
1,6-Diisopropyl-3,8-dibromopyrene Usage And Synthesis
Uses1,6-Diisopropyl-3,8-dibromopyrene can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.
SynthesisSynthesis_869340-02-3
In a three-neck round bottom flask, dissolve 2.86 g (10 mmol) of Intermediate-1 in 40 mL of CCl4. Dropped in a round bottom flask 4.00 g (25 mol) of Br 2 and 30 mL of CCl 4 were added to the funnel, and the mixture was slowly dropped into a round bottom flask over 4 hours N2 is injected to remove HBr generated. When dropping is completed, stirring is carried out under N2 air flow for 1 hour When the reaction was terminated, the resulting precipitate was filtered as it was, and the precipitate was recrystallized using toluene to give (2.8 g, 58%).
1,6-Diisopropyl-3,8-dibromopyrene Preparation Products And Raw materials

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