9-VINYLANTHRACENE

9-VINYLANTHRACENE Basic information

Product Name:	9-VINYLANTHRACENE
Synonyms:	9-VINYLANTHRACENE;10-vinylanthracene;9-Ethenylanthracen;9-Vinylanthracene 97%;9-Vinylanthracene,97%;9-vinyl-anthracene radical cation;9-Ethenyl anthracene;Anthracene, 9-ethenyl-
CAS:	2444-68-0
MF:	C16H12
MW:	204.27
EINECS:	219-486-2
Product Categories:	Styrenes;Photoluminescent Materials > Fluorescent MonomersPolymer Science;Monomers;Photonic and Optical Materials;Styrene and Functionalized Styrene MonomersPolymer Science;Vinyl Halides, Amines, Amides, and Other Vinyl Monomers
Mol File:	2444-68-0.mol

9-VINYLANTHRACENE Chemical Properties

Melting point	62-65 °C (lit.)
Boiling point	61-66 °C/10 mmHg (lit.)
density	1.1570 (estimate)
refractive index	1.5000 (estimate)
Fp	61-66°C/10mm
storage temp.	Store below +30°C.
form	powder to crystal
color	White to Yellow to Orange
BRN	2041641
CAS DataBase Reference	2444-68-0(CAS DataBase Reference)

Safety Information

Safety Statements	22-24/25
WGK Germany	3
HS Code	2902 90 00

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English
ALFA	English

9-VINYLANTHRACENE Usage And Synthesis

Chemical Properties	yellow to green crystalline solid
Uses	9-Vinylanthracene (cas# 2444-68-0) is a compound useful in organic synthesis.
Synthesis Reference(s)	The Journal of Organic Chemistry, 56, p. 4035, 1991 DOI: 10.1021/jo00012a043 Synthesis, p. 319, 1981
Purification Methods	Purify it by vacuum sublimation. It has also been purified by chromatography on silica gel with cyclohexane as eluent, and recrystallised from EtOH [Werst et al. J Am Chem Soc 109 32 1987]. [Beilstein 5 IV 2415.]

9-VINYLANTHRACENE Preparation Products And Raw materials

Raw materials

Ethanol-->Methanol-->Tetrahydrofuran-->Acetic acid-->N,N-Dimethylformamide-->Phosphorus oxychloride-->Aluminum chloride-->Sodium borohydride-->Iodomethane-->p-Toluenesulfonic acid-->Acetyl chloride-->Sodium acetate-->Sodium azide-->Triphenylphosphine-->Tosyl chloride-->Oxalyl chloride-->Potassium tert-butoxide-->1,2-Dichloroethane-->Anisole-->1,2-Dichlorobenzene-->Methyl bromide-->Potassium bisulfate-->Anthracene-->DBU-->2-Pyrrolidinone-->Anthrone-->3-Chloro-1-propanol-->Vinylmagnesium bromide-->9-Anthraldehyde

Preparation Products

polyvinyl anthracene

3-(9-ANTHRYL)-1-(2-FURYL)PROP-2-EN-1-ONE 9,10-Epoxy-9,10-dihydrobenz(j)aceanthrylene 3-(9-ANTHRYL)-1-(4-METHOXYPHENYL)PROP-2-EN-1-ONE 3-(9-ANTHRYL)-1-(4-METHYLPHENYL)PROP-2-EN-1-ONE aceanthrylene naphtho(2,1,8-hij)acephenanthrylene 3-(9-ANTHRYL)-1-(4-BROMOPHENYL)PROP-2-EN-1-ONE ISOVIOLANTHRENE (5E)-5-(9-ANTHRYLMETHYLENE)-3-(4-METHOXYPHENYL)-2-THIOXO-1,3-THIAZOLIDIN-4-ONE AKOS B004032 3-(9-ANTHRYL)-1-(2,4-DIMETHOXYPHENYL)PROP-2-EN-1-ONE 3-(9-ANTHRYL)-1-(3-BROMOPHENYL)PROP-2-EN-1-ONE 3-(9-ANTHRYL)-1-(3-METHOXYPHENYL)PROP-2-EN-1-ONE 3-(9-ANTHRYL)-1-(3-METHYLPHENYL)PROP-2-EN-1-ONE benz(e)aceanthrylene benz(j)aceanthrylene 3-(9-ANTHRYL)-1-(2-NAPHTHYL)PROP-2-EN-1-ONE 9-(2-nitrovinyl)anthracene

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