5-Bromo-2-methoxyphenol

5-Bromo-2-methoxyphenol Basic information

Product Name:	5-Bromo-2-methoxyphenol
Synonyms:	5-BROMO-2-METHOXYPHENOL;3-HYDROXY-4-METHOXYBROMOBENZENE;5-Brom-2-methoxy-phenol;5-Bromo-2-methoxyphenol ,99%;5-Bromoguaiacol (OH=1);4-Bromo-2-hydroxyanisole;Phenol, 5-broMo-2-Methoxy-;4-Bromo-2-hydroxyanisole, 5-Bromoguaiacol
CAS:	37942-01-1
MF:	C7H7BrO2
MW:	203.03
EINECS:	609-492-7
Product Categories:	blocks;Bromides
Mol File:	37942-01-1.mol

5-Bromo-2-methoxyphenol Chemical Properties

Melting point	64-70
Boiling point	150 °C / 20mmHg
density	1.585±0.06 g/cm3(Predicted)
storage temp.	Inert atmosphere,Room Temperature
form	powder to crystal
pka	9.01±0.10(Predicted)
color	White to Almost white
InChIKey	OLSJHVZRUFFIPL-UHFFFAOYSA-N
CAS DataBase Reference	37942-01-1(CAS DataBase Reference)

Safety Information

Hazard Codes	Xi
Risk Statements	20/21/22-36/37/38
Safety Statements	26-36/37/39
Hazard Note	Irritant/Store Cold
HazardClass	IRRITANT
HS Code	29095000

MSDS Information

5-Bromo-2-methoxyphenol Usage And Synthesis

Chemical Properties	White to off-white crystal
Uses	The 5-Bromo-2-methoxyphenol is the important intermediate of producing depressor aliskiren.
Synthesis	The 5-bromo-2-methoxyphenol is synthesized by virtue of three steps of reactions as follows: by taking o-methoxyphenol as the raw materials, performing acetylation protection on the phenolic hydroxyl by use of acetic anhydride, and then performing bromination by use of bromine under the catalysis of iron powder, and finally performing deacetylation.

5-Bromo-2-methoxyphenol Preparation Products And Raw materials

Raw materials	Phenol, 2-methoxy-, methanesulfonate -->Trifluoroacetic acid 2-methoxyphenyl ester-->2-METHOXYPHENYL BENZOATE-->5-Bromo-2-methoxyphenylacetate-->2-METHOXYPHENYL ACETATE-->5-Bromo-2-methoxyphenyl methanesulfonate-->5-Bromo-2-anisaldehyde-->2,4-DIBROMOANISOLE-->Guaiacol-->4-Bromoanisole
Preparation Products	2,8-dibromooxanthrene-->3-(Benzyloxy)-4-methoxyphenylboronic acid-->2-BROMO-6-METHOXY-PHENOL

4-((1S)-1-AMINOPROPYL)-2-BROMO-6-METHOXYPHENOL 4-(2-amino-1-hydroxyethyl)-2-bromo-6-methoxyphenol DL-6'-BROMOLAUDANOSIN 2-BROMO-4,5-DIMETHOXYPHENYLACETIC ACID 2-Bromo-4,5-dimethoxyphenylacetonitrile METHYL 6-BROMO-3,4-DIMETHOXYBENZOATE 2,3-DIBROMO-6-HYDROXY-5-METHOXY-BENZALDEHYDE 2-BROMO-4,5-DIMETHOXYCINNAMIC ACID METHOXYPHENOL, PARA-(SG) 1-BROMO-4,5-DIMETHOXY-2-NITROBENZENE 6-BROMO-2-HYDROXY-3-METHOXYBENZALDEHYDE 2-((1R)-1-AMINO-2-METHYLPROPYL)-4-BROMO-6-METHOXYPHENOL 2-((1R)-1-AMINOPROPYL)-4-BROMO-6-METHOXYPHENOL 2-((1R)AMINOCYCLOPROPYLMETHYL)-6-BROMO-4-METHOXYPHENOL 2-BROMO-6-HYDROXY-5-METHOXY-3-NITRO-BENZALDEHYDE 2-(2-AMINO-3,4-DIHYDRO[1,3,5]TRIAZINO[1,2-A]BENZIMIDAZOL-4-YL)-4-BROMO-6-METHOXYPHENOL 5-Bromo-2-methoxyphenol 2-((1R)-1-AMINOBUTYL)-4-BROMO-6-METHOXYPHENOL

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