ChemicalBook Product Catalog Chemical Reagents Organic reagents Imide N-AMINOPHTHALIMIDE

N-AMINOPHTHALIMIDE

N-AMINOPHTHALIMIDE Basic information
Product Name:N-AMINOPHTHALIMIDE
Synonyms:Aminophthalimidetech;2-AMINOISOINDOLINE-1,3-DIONE;N,N-PHTHALOYLHYDRAZINE, UNSYM;N-AMINOPHTHALIMIDE;SPECS AQ-344/40414632;N-AMINOPHTHALIMIDE, TECH., 90%;2-aminoisoindole-1,3-dione;2-aminoisoindoline-1,3-dione 98%
CAS:1875-48-5
MF:C8H6N2O2
MW:162.15
EINECS:217-505-9
Product Categories:Building Blocks;Carbonyl Compounds;N-Substituted Maleimides, Succinimides & Phthalimides;Chemical Synthesis;Hydrazides;Organic Building Blocks;N-Substituted Phthalimides
Mol File:1875-48-5.mol
N-AMINOPHTHALIMIDE Structure
N-AMINOPHTHALIMIDE Chemical Properties
Melting point 200-202 °C(lit.)
Boiling point 288.82°C (rough estimate)
density 1.3264 (rough estimate)
refractive index 1.5770 (estimate)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Solubility in hot methanol almost transparent.
pka-1.73±0.20(Predicted)
form powder to crystal
color White to Light yellow
BRN 383756
CAS DataBase Reference1875-48-5(CAS DataBase Reference)
Safety Information
Hazard Codes Xn
Risk Statements 36/37/38-42/43
Safety Statements 22-26-36/37-45
WGK Germany 3
F 9
HS Code 29251900
MSDS Information
ProviderLanguage
SigmaAldrich English
ACROS English
ALFA English
N-AMINOPHTHALIMIDE Usage And Synthesis
Chemical Propertieswhite to off-white crystalline powder
UsesIt is employed in the aziridination of chiral N-enoyl sultams. It is also used in the synthesis of n-phthalimidoaziridines
UsesN-Aminophthalimide was employed in the aziridination of chiral N-enoyl sultams. It was also used in the synthesis of n-phthalimidoaziridines.
Purification MethodsThe imide has been recrystallised from 96% EtOH (solubility is ~2% at boiling temperature) to form a yellow solution. It sublimes in vacuo at ca 150o. It solidifies after melting, and remelts at 338-341o (see phthalhydrazide in “Heterocyclic Compounds, Chapter 4”). [Beilstein 22/11 V 122.]
N-AMINOPHTHALIMIDE Preparation Products And Raw materials
Raw materialsN-(3-BUTYNYL)PHTHALIMIDE-->3-BUTYN-1-AMINE HYDROCHLORIDE
2-(2-toluidino)-1H-isoindole-1,3(2H)-dione 2-(5-[(4-CHLOROPHENYL)METHYLENE]-4-OXO-2-THIOXO-1,3-THIAZOLAN-3-YL)-1H-ISOINDOLE-1,3(2H)-DIONE 2-(4-TOLUIDINO)-1H-ISOINDOLE-1,3(2H)-DIONE 1H-Isoindole-1,3(2H)-dione, 2-(((3-methoxyphenyl)methylene)amino)- 2-(4-CHLOROANILINO)-1H-ISOINDOLE-1,3(2H)-DIONE 2-(5-[(DIMETHYLAMINO)METHYLENE]-4-OXO-2-THIOXO-1,3-THIAZOLAN-3-YL)-1H-ISOINDOLE-1,3(2H)-DIONE 2-[(6-CHLORO-2-PYRIDINYL)AMINO]-1H-ISOINDOLE-1,3(2H)-DIONE 2-(2,4-DICHLOROANILINO)-1H-ISOINDOLE-1,3(2H)-DIONE 2-(5-[(4-FLUOROPHENYL)METHYLENE]-4-OXO-2-THIOXO-1,3-THIAZOLAN-3-YL)-1H-ISOINDOLE-1,3(2H)-DIONE 2-[(2-CHLORO-5-NITROBENZYLIDENE)AMINO]ISOINDOLINE-1,3-DIONE 2-anilino-1H-isoindole-1,3(2H)-dione 2-(4-OXO-2-THIOXO-1,3-THIAZOLAN-3-YL)-1H-ISOINDOLE-1,3(2H)-DIONE 2-(4H-1,2,4-TRIAZOL-4-YL)-1H-ISOINDOLE-1,3(2H)-DIONE SALOR-INT L164585-1EA N-PHTHALIMIDOPHTHALIMIDE 2-(4-FLUOROANILINO)-1H-ISOINDOLE-1,3(2H)-DIONE 2-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]AMINO)-1H-ISOINDOLE-1,3(2H)-DIONE N-AMINOPHTHALIMIDE
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