P-TOLUAMIDE

P-TOLUAMIDE Basic information
Product Name:P-TOLUAMIDE
Synonyms:p-Toluamide 99%;p-Toluamide;Cladribine Impurity F (4-Methylbenzamide);Mettler-Toledo Calibration substance ME 30130597, p-Toluamide;4-methyl-benzamid;Benzamide,4-methyl-;p-Tolylamide;Tolylsαureamid
CAS:619-55-6
MF:C8H9NO
MW:135.16
EINECS:210-600-6
Product Categories:Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts;AMIDE;Benzene derivatives;Amides;Building Blocks;Carbonyl Compounds;Chemical Synthesis;Organic Building Blocks
Mol File:619-55-6.mol
P-TOLUAMIDE Structure
P-TOLUAMIDE Chemical Properties
Melting point 161-163 °C (lit.)
Boiling point 248.86°C (rough estimate)
density 1.1031 (rough estimate)
refractive index 1.5635 (rough estimate)
storage temp. Sealed in dry,Room Temperature
solubility soluble in Methanol
pka16.21±0.50(Predicted)
form powder to crystal
color White to Almost white
Sensitive Air Sensitive
BRN 774353
CAS DataBase Reference619-55-6(CAS DataBase Reference)
EPA Substance Registry SystemBenzamide, 4-methyl- (619-55-6)
Safety Information
Hazard Codes Xn
Risk Statements 22-36
Safety Statements 24/25-26
WGK Germany 3
RTECS CV5570150
TSCA Yes
HS Code 29242990
MSDS Information
ProviderLanguage
ACROS English
ALFA English
P-TOLUAMIDE Usage And Synthesis
Chemical Propertieswhite crystalline powder or needles
Usesp-Toluamide Mettler-Toledo calibration substance ME 30130597 is used to calibrate Mettler-Toledo melting point instruments.
Usesp-Toluamide has been used in preparation of p-toloyl isocyanate.
Uses4-Methylbenzamide is used in preparation of high efficiency nitriding reagents.
DefinitionChEBI: P-toluamide is a member of benzamides.
Synthesis Reference(s)The Journal of Organic Chemistry, 20, p. 1448, 1955 DOI: 10.1021/jo01127a025
General DescriptionMettler-Toledo calibration substance ME 30130597, p-toluamide is an analytical standard, ideal for use in the routine calibration of Mettler-Toledo melting point instrument. Its value is measured as a mean of 6 to 12 iterations using a Mettler-Toledo MP70 Excellence instrument that is calibrated with primary standards. The melting point determination is carried out by Capillary method in accordance with European Pharmacopeia (2.2.14.)
P-TOLUAMIDE Preparation Products And Raw materials
Preparation Productsp-Tolyl isocyanate-->4-METHYL-3-NITROBENZAMIDE-->2,4,6-trip-tolyl-1,3,5-triazine-->4-Methylbenzamide oxime-->4-METHYL(THIOBENZAMIDE)-->2-Bromo-4-methylaniline-->N-(2-Methoxyphenyl)-4-MethylbenzaMide, 97%-->4-(difluoromethyl)benzamide-->Benzamide, N-formyl-4-methyl- (9CI)
4-AMIDINOBENZAMIDE HYDROCHLORIDE AURORA 1033 p-Toluamide, N,N-dicyclohexyl-3-(3,3-dimethyltriazeno)- (4-TERT-BUTYL-BENZOYLAMINO)-ACETIC ACID N,N-DIETHYLORTHO-TOLUAMIDE N-ETHYL-META-TOLUAMIDE 4-(Allyloxy)-5-propyl-N,N,3-triethyl-o-toluamide N-Ethyl-m-toluamide N-(5,5-Dimethyl-2-oxotetrahydro-3-furyl)-alpha,alpha,alpha-trifluoro-p -toluamide N-isopropyl-alpha-(2-methylhydrazo)-4-toluamide 4,4'-BISBENZHYDRAZIDE N,N-(Diethyl-d10)-m-toluamide 4-CYANOBENZAMIDE P-TOLUIC HYDRAZIDE N,N-Diisopropyl-p-toluamide N-Phenyl-p-toluamide N,N-DIETHYL-META-TOLUAMIDE-N-OXIDE AURORA 2242

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