|
| | SMILAGENIN Basic information |
| Product Name: | SMILAGENIN | | Synonyms: | 5BETA,20ALPHA,22ALPHA,25D-SPIRANOSTAN-3BETA-OL;5-BETA, 20-ALPHA, 22-ALPHA, 25D-SPIROSTAN-3-BETA-OL;25R,5BETA-SPIROSTAN-3BETA-OL;(25R)-SPIROSTAN-3BETA-OL;16,22:22,26-BIS(EPOXY)CHOLESTAN-3BETA-OL;SMILAGENIN;(25r)-spirostan-3β-ol;(25R)-Spirostan-3β-ol, 16,22:22,26-Bis(epoxy)cholestan-3β-ol | | CAS: | 126-18-1 | | MF: | C27H44O3 | | MW: | 416.64 | | EINECS: | 204-775-8 | | Product Categories: | Steroids | | Mol File: | 126-18-1.mol |  |
| | SMILAGENIN Chemical Properties |
| Melting point | ~185 °C | | alpha | D25 -69° (c = 0.5 in chloroform) | | Boiling point | 474.91°C (rough estimate) | | density | 1.0362 (rough estimate) | | refractive index | 1.4700 (estimate) | | storage temp. | Store at -20°C | | solubility | Ethanol: ≥ 10 mg/mL (24.00 mM); DMSO: < 1 mg/mL (insoluble or slightly soluble) | | pka | 15.14±0.70(Predicted) |
| | SMILAGENIN Usage And Synthesis |
| Definition | ChEBI: An oxaspiro compound that is(5beta,25R)-spirostan substituted by a beta-hydroxy group at position 3. | | Purification Methods | Chromatograph smilagenin on active Al2O3 and elute with *C6H6, then recrystallise it from Me2CO, aqueous EtOH (m 187-188o) or MeOH. The acetate crystallises from MeOH with m 152o and [] D 25 -59.6o, [] 546 25 –68.9o (c 0.25, CHCl3). [Askew J Chem Soc 1399 1936 and 1402 1936, Scheer et al. J Am Chem Soc 77 6411955, Beilstein 19 III/IV 826.] |
| | SMILAGENIN Preparation Products And Raw materials |
|
