9,10-Dibromoanthracene

9,10-Dibromoanthracene Basic information
Product Name:9,10-Dibromoanthracene
Synonyms:9,10-Dibromoanthracene99%;9,I O-Dibromanthracen;9,10-DIBROMO ANTHRACENEN;9,10-Dibromoanthracene,96%;Anthracene,9,10-dibromo-;ms-Dibromoanthracene;9,10-DIBROMOANTHRACENE;9,10-DIRBOMOANTHRACENE
CAS:523-27-3
MF:C14H8Br2
MW:336.02
EINECS:208-342-4
Product Categories:Miscellaneous;Aromatic Compounds;Electronic Chemicals;Anthracenes;Anthracene series;Aryl;C13 to C37+;Halogenated Hydrocarbons;C13 to C37+;Building Blocks;Chemical Synthesis;Halogenated Hydrocarbons;Organic Building Blocks;OLED materrials;OLED
Mol File:523-27-3.mol
9,10-Dibromoanthracene Structure
9,10-Dibromoanthracene Chemical Properties
Melting point 223-224 °C (lit.)
Boiling point 342.21°C (rough estimate)
density 1.7167 (estimate)
refractive index 1.6300 (estimate)
storage temp. Sealed in dry,Room Temperature
solubility Chloroform
form Fluffy Powder
color Yellow to yellow-green
Water Solubility Soluble in water.
Merck 14,3018
BRN 1912109
InChIKeyBRUOAURMAFDGLP-UHFFFAOYSA-N
CAS DataBase Reference523-27-3(CAS DataBase Reference)
NIST Chemistry ReferenceAnthracene, 9,10-dibromo-(523-27-3)
EPA Substance Registry SystemAnthracene, 9,10-dibromo- (523-27-3)
Safety Information
Hazard Codes Xi,N
Risk Statements 36/37/38-50/53
Safety Statements 37/39-26-61-60-36
RIDADR UN 3077
WGK Germany 3
TSCA Yes
HS Code 29039990
MSDS Information
ProviderLanguage
9,10-Dibromoanthracene English
ACROS English
ALFA English
9,10-Dibromoanthracene Usage And Synthesis
Chemical PropertiesYellow to yellow-green fluffy powder. Melting point 226°C. It can be sublimated and oxidized to generate anthraquinone. Soluble in hot benzene and hot toluene, slightly soluble in alcohol, ether and cold benzene, insoluble in water.
Uses9,10-Dibromoanthracene is a dibrominated polycyclic aromatic hydrocarbon (PAH). 9,10-Dibromoanthracene is often used as an energy acceptor and activator in reactions that produce chemiluminescence.
Uses9,10-Dibromoanthracene is an important raw material and intermediate used in organic synthesis, pharmaceuticals and agrochemicals.
Preparation9,10-Dibromoanthracene is synthesized by the bromination of anthracene. The bromination reaction is carried out at room temperature using carbon tetrachloride as a solvent. Using 80-85% anthracene as raw material, adding bromine to react for half an hour, the yield is 83-88%.
523-27-3.png
Purification MethodsRecrystallise it from toluene, xylene or CCl4 (yellow needles), and sublime it in a vacuum [Johnston et al. J Am Chem Soc 109 1291 1987]. [Heilbron & Heaton Org Synth Coll Vol I 207 1941, Beilstein 5 H 665.]
9,10-Dibromoanthracene-2-sulfonyl Chloride 1,2-DIBROMOETHYLENE 2,4-DIBROMOPENTANE 1,4,9,10-TETRABROMO-ANTHRACENE 2-PHENYL-9,10-(DIBROMOANTHRACENE) 9,10-Dibromoanthracene Α,Β-DIBROMOPROPIONIC ACID 9,10-DIBROMO-2-METHYLANTHRACENE 2,2-Bis(bromomethyl)propane-1,3-diol 1,2-Dibromopropane 9,10-DIBROMOANTHRACENE-2-SULFONIC ACID 2-TERTBUTYL-9,10-DIBROMOANTHRACENE 1,3-Dibromo-5,5-dimethylhydantoin 1,3,9,10-TETRABROMO-ANTHRACENE 9,10-Dibromoanthracene-2-sulfonic Acid, Sodium Salt meso-2,3-Dibromosuccinic acid DBDCB 1,3-Bis(bromomethyl)benzene

Email:[email protected] [email protected]
Copyright © 2024 Mywellwork.com All rights reserved.