ChemicalBook Product Catalog Organic Chemistry Amides 4-methoxy-3-methylaniline

4-methoxy-3-methylaniline

4-methoxy-3-methylaniline Basic information
Product Name:4-methoxy-3-methylaniline
Synonyms:4-AMino-2-Methylanisole[4-Methoxy-3-Methylaniline];3-Methyl-4-methoxybenzenamine;4-AMINO-2-METHYLANISOLE;4-METHOXY-3-METHYLANILINE;3-Methyl-4-methoxyaniline;4-methoxy-3-methylbenzenamine;BenzenaMine, 4-Methoxy-3-Methyl-;4-AMINO-24-AMINO-2-METHYLANISOLE-METHYLANISOLE
CAS:136-90-3
MF:C8H11NO
MW:137.18
EINECS:
Product Categories:
Mol File:136-90-3.mol
4-methoxy-3-methylaniline Structure
4-methoxy-3-methylaniline Chemical Properties
Melting point 57-60℃
Boiling point 252.03°C (rough estimate)
density 1.0630 (rough estimate)
refractive index 1.5360 (estimate)
storage temp. Keep in dark place,Inert atmosphere,Room temperature
solubility Chloroform (Slightly), Methanol (Slightly)
form Solid
pka5.32±0.10(Predicted)
color Dark Red to Black
Safety Information
Hazard Codes Xn
Risk Statements 20/21/22-36/37/38
Safety Statements 26-36/37/39
WGK Germany 3
HS Code 2922290090
MSDS Information
4-methoxy-3-methylaniline Usage And Synthesis
Uses4-Methoxy-3-methylaniline is used in preparation of triamine pyrimidine derivatives as antitumor agents.
SynthesisThe synthesis of 4-methoxy-3-methylaniline is as follows:
4-Methoxy-3-methyl-phenylamine10% Palladium on carbon (10% Pd/C) (1.5 g) was added to a solution of 1 -methoxy-2- methyl-4-nitrobenzene (9.5 g, 57 mmol) in methanol (100 ml_). The mixture was stirred under a hydrogen atmosphere (1 atm.) at room temperature for 16 h. The mixture was filtered through a pad of CELITE and the filtrate was evaporated in vacuo to yield 4- methoxy-3-methylphenylamine (8.0 g, 57 mmol, 100%).
synthesis of 4-methoxy-3-methylaniline.png
4-tert-Butyl-2,6-dinitro-3-methoxytoluene 6-ACETAMIDOCOUMARIN 2-FORMYL-4-NITROPHENOXYACETIC ACID 5-AMINO-2-METHOXYBENZOTRIFLUORIDE 2-TETRAFLUOROETHOXY-5-NITROTOLUENE METHYL 2,6-DIMETHOXY-3-NITROBENZOATE 2-METHOXY-5-NITROBENZYL BROMIDE 2,3-DIMETHYL-4-NITROANISOLE 2-METHOXY-5-NITROBENZOTRIFLUORIDE 2,6-DIMETHYL-4-NITROANISOLE 6-nitrocoumarin 4,5-DIHYDRO-1,3-BENZODIOXINE-6-AMINE EOSIN B 2-AMINO-6 H-DIBENZO[B,D]PYRAN-6-ONE 4-AMINO-2-ISOPROPYLANISOL 2-methoxy-5-nitrobenzonitrile 2,6-DIMETHOXY-3-NITROBENZOIC ACID 5-METHOXY-2-NITRO-P-TOLUIDINE
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