1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Basic information
Product Name:1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene
Synonyms:1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-Methylbenzene 4-(3-Acryloyloxypropyloxy)-benzoesure -2-Methyl-1, 4-phenylester;2-Methyl-1,4-phenylene-bis[4[3(acryloyloxy)propyloxy]benzoate];4-(3-Acryloyloxypropyloxy)benzoic acid 2-methyl-1,4-phenylene ester;2-Methyl-1,4-phenylene bis(4-(3-(acryloyloxy)propoxy)benzoate);Benzoic acid, 4-[3-[(1-oxo-2-propenyl)oxy]propoxy]-,2-methyl-1,4-phenylene ester;4- (3-acryloyloxy-propoxy) benzoic acid 2-methyl-1,4-phenylene ester;1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenze;4-(3-Acryloyloxypropyloxy)-benzoesure 2-methyl-1, 4-phenylester
CAS:174063-87-7
MF:C33H32O10
MW:588.6
EINECS:425-560-7
Product Categories:
Mol File:174063-87-7.mol
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Structure
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Chemical Properties
Boiling point 733.5±60.0 °C(Predicted)
density 1.219
vapor pressure 0.003Pa at 25℃
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form powder
color White
Water Solubility 5.3μg/L at 20℃
LogP5.3 at 40℃
Safety Information
HS Code 2917399590
MSDS Information
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Usage And Synthesis
Chemical PropertiesWhite to Almost white powder to crystal
Application1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is one of numerous organic compounds composing American Elements's comprehensive catalog of life science products.
Flammability and ExplosibilityNotclassified
SynthesisThe synthesis of 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is as follows:Stirrer, was added methanesulfonyl chloride 5.00 g (43.6 mmol) and tetrahydrofuran 10mL the reactor having a thermometer and two dropping device. Ice-cold while each by dropping a tetrahydrofuran solution 30mL of formula tetrahydrofuran solution 60mL and triethylamine 5.25g of (I-3-1) represented by the compound 12.9g (44.1 mmol) of (51.9 mmol) from device (equation (solution of the compound represented by I-3-1)) :( triethylamine solution) = 2: were added dropwise simultaneously with one of the drip rate.After stirring for 1 hour while cooling with ice, it was added 4-dimethylaminopyridine 2.64 g (21.6 mmol) and 2- (4-hydroxyphenyl) ethanol 2.69 g (19.4 mmol).With ice-cooling was added dropwise triethylamine 5.25g (51.9 mmol).After stirring for 7 hours, the solvent was distilled off and treated added for liquid separation dichloromethane and 5% hydrochloric acid.After the organic layer was washed with brine neutralization, and purified by column chromatography (silica gel) and reprecipitated (dichloromethane / methanol) to give the compound 12.2g of formula (I-3).82% yield, had a purity of 99.63%.

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1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Preparation Products And Raw materials
Raw materials4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID-->2-Methylhydroquinone
L-Alanyl-L-Glutamine 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene 4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID

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