5-Chloro-2-methoxyaniline

5-Chloro-2-methoxyaniline Basic information

Product Name:	5-Chloro-2-methoxyaniline
Synonyms:	2-Amino-4-chioroanisole;5-chloro-2-methoxy-benzenamin;C.I.37120(base);C.I.Azoic Diazo Component 10(base);Tulabase Fast Red R;5-Chloro-o-anisidine 4-Chloro-2-aminoanisole 2-Amino-4-chloroanisole;5-Chloro-o-anisidine,98%;5-Chloro-2-methoxyaniline 98%
CAS:	95-03-4
MF:	C7H8ClNO
MW:	157.6
EINECS:	202-385-2
Product Categories:	API Intermediate;Anilines, Aromatic Amines and Nitro Compounds;Intermediates of Dyes and Pigments
Mol File:	95-03-4.mol

5-Chloro-2-methoxyaniline Chemical Properties

Melting point	81-83 °C(lit.)
Boiling point	135 °C (5.85078 mmHg)
density	1.1760 (rough estimate)
refractive index	1.5430 (estimate)
Fp	136 °C
storage temp.	Amber Vial, -20°C Freezer, Under inert atmosphere
solubility	Chloroform (Slightly), DMSO (Slightly)
pka	3.48±0.10(Predicted)
form	Solid
color	Pale Grey to Light Grey
BRN	879161
Stability:	Light Sensitive
CAS DataBase Reference	95-03-4(CAS DataBase Reference)
EPA Substance Registry System	Benzenamine, 5-chloro-2-methoxy- (95-03-4)

Safety Information

Hazard Codes	Xn,Xi
Risk Statements	20/21/22-36/37/38
Safety Statements	26-36/37
RIDADR	UN 2233 6.1/PG 3
WGK Germany	3
TSCA	Yes
HazardClass	6.1
PackingGroup	III
HS Code	29222990

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English
ALFA	English

5-Chloro-2-methoxyaniline Usage And Synthesis

Chemical Properties	Off-white to tan crystalline powder or flakes
Uses	5-Chloro-2-methoxybenzenamine is used in preparation of appetite-modulating molecules.
Preparation	4-Chloro-1-methoxy-2-nitrobenzene reduction.
Purification Methods	Purify the aniline by steam distillation and recrystallisation from H2O or 40% aqueous EtOH. The N-acetate forms needles from hot H2O with m 104o, the N-benzoyl derivative forms needles from aqueous EtOH with m 77-78o, and the picrate has m 194o(dec). [Raiford & Colbert J Am Chem Soc 48 2657 1926, Beilstein 13 IV 879.]

5-Chloro-2-methoxyaniline Preparation Products And Raw materials

Raw materials	Iron-->o-Anisidine-->Iron oxide-->PETROLEUM ETHER-->63083-96-5-->4,5-Dichloro-2-Methoxyaniline-->4-Chloro-2-nitroanisole-->Phenol-->Ethanol-->4-Chlorophenol-->4-Chloroanisole
Preparation Products	4-CHLORO-2-FLUOROANISOLE-->4-CHLORO-2-ANISIDINE HYDROCHLORIDE-->2-Chloro-5-methoxyaniline-->SOLVENT VIOLET 2-->disodium hydrogen bis[5-[(5-chloro-2-hydroxyphenyl)azo]-6-hydroxynaphthalene-2-sulphonato(3-)]chromate(3-)

Chlorzoxazone 1-chloro-2,4-dimethoxy-5-nitrobenzene 5-Chloro-2-(2-chlorophenoxy)aniline 5-CHLORO-2-METHOXYPHENYL ISOCYANATE FAST RED RC SALT 1-(2-bromoethoxy)-4-chloro-2-nitrobenzene 2,4-DIMETHOXY-5-CHLORO PHENYL UREA N-(5-Chloro-2-methoxyphenyl)-3-oxobutanamide 5-Chloro-2,4-dimethoxyaniline 5-CHLORO-2-METHOXYANILINE HYDROCHLORIDE,P-CHLORO-O-AMINOANISOLE HCL 5-CHLORO-2,4-DIMETHOXYPHENYL ISOCYANATE 5-Chloro-2-methoxyaniline 4-Chloro-1-(4-chlorophenoxy)-2-nitrobenzene N-(5-CHLORO-2,4-DIMETHOXYPHENYL)-N'-METHYLTHIOUREA 2-AMINO-4,4'-DICHLORODIPHENYL ETHER N-(2-Hydroxynaphthoyl)-2,4-dimethoxy-5-chloroanilide 4-Chloro-2-nitroanisole 5-chloro-2-(4-chlorophenoxy)-N,N-dimethylaniline

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