3-HYDROXYBENZOPHENONE

3-HYDROXYBENZOPHENONE Basic information

Product Name:	3-HYDROXYBENZOPHENONE
Synonyms:	(3-Hydroxyphenyl)(phenyl)methanone;Methanone, (3-hydroxyphenyl)phenyl-;M-HYDROXYBENZOPHENONE;3-Hydroxybenzophenone,99%;3-HYDROXYBENZOPHENONE;M-BENZOYL PHENOL
CAS:	13020-57-0
MF:	C13H10O2
MW:	198.22
EINECS:	235-879-1
Product Categories:	Aromatic Benzophenones & Derivatives (substituted);Linkers for Solid Phase Synthesis;Benzophenone;Organic Photoinitiators;Polymerization Initiators
Mol File:	13020-57-0.mol

3-HYDROXYBENZOPHENONE Chemical Properties

Melting point	113-115 °C (lit.)
Boiling point	295.53°C (rough estimate)
density	1.1184 (rough estimate)
refractive index	1.5954 (estimate)
storage temp.	Inert atmosphere,Room Temperature
solubility	Soluble in Chloroform, DCM. Ethyl Acetate.
form	Solid
pka	9.18±0.10(Predicted)
color	White
λmax	315nm(EtOH)(lit.)
CAS DataBase Reference	13020-57-0(CAS DataBase Reference)
NIST Chemistry Reference	M-hydroxybenzophenone(13020-57-0)

Safety Information

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-37/39-36
WGK Germany	3
RTECS	PC4959730
HazardClass	IRRITANT
HS Code	29145090

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English
ALFA	English

3-HYDROXYBENZOPHENONE Usage And Synthesis

Chemical Properties	light beige to brown-grey crystalline powder
Uses	3-Hydroxybenzophenone is a benzophenone metabolite with potential estrogenic and anti-androgenic activity. is a more attractive hydrogen bonding co-material for MCPBA, as the 3-hydroxyl group is unable to form an intramolecular hydrogen bond. It is commonly used as a radical and cationic photo initiators.
Preparation	Preparation by aromatization of 5-benzoyl-2- cyclohexenone, ? in the presence of 10% Pd/C in refluxing xylene for 6 h (60%) ? in the presence of lithium bromide and cupric bromide in refluxing acetonitrile for 1 h (75%).

3-HYDROXYBENZOPHENONE Preparation Products And Raw materials

Raw materials	3-Hydroxy-n-methoxy-n-methylbenzamide-->3-METHOXYBENZOPHENONE-->3-IODOBENZOPHENONE-->Phenyl trifluoromethanesulfonate-->3-Bromobenzophenone-->3-METHOXYBENZOYL CHLORIDE-->3-Hydroxybenzoic acid-->Phenylboronic acid-->3-Hydroxybenzaldehyde-->Benzophenone-->4-Hydroxybenzophenone
Preparation Products	2-Hydroxybenzophenone-->Phthalide

6,7-DICHLORO-1,4-DIHYDROXYANTHRAQUINONE, 97 Alizarin Red S PURPURIN ISLANDICIN Emodin Rhein NICKEL ALIZARINATE 1,2,5,8-TETRAHYDROXYANTHRAQUINONE 1,8-Dihydroxyanthraquinone 2,6-DIHYDROXYANTHRAQUINONE 2,3,3',4'-TETRAMETHOXYBENZOPHENONE 2-HYDROXY-9-FLUORENONE FRANGULIN B FRANGULIN A 1,5-DIAMINO-4,8-DIHYDROXYANTHRAQUINONE CATENARIN 1,5-DIHYDROXYANTHRAQUINONE 1,2,3,4-TETRAMETHOXY-10-METHYLACRIDONE

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