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| 1-Methylcyclopentyl methacrylate Basic information |
Product Name: | 1-Methylcyclopentyl methacrylate | Synonyms: | 1-Methylcyclopentyl methacrylate;MCPMA 1-Methylcyclopentyl methacrylate;1-Methylcyclopentyl methacrylate MCPMA ArF monomers;1-Methylcyclopentyl methacrylate 178889-45-7;2-Propenoic acid, 2-methyl-, 1-methylcyclopentyl ester 178889-45-7;2-Propenoic acid, 2-methyl-, 1-methylcyclopentyl ester;1-Methylcyclopentyl Methacrylate (stabilized with MEHQ);Methacrylic Acid 1-Methylcyclopentyl Ester | CAS: | 178889-45-7 | MF: | C10H16O2 | MW: | 168.23 | EINECS: | | Product Categories: | | Mol File: | 178889-45-7.mol | |
| 1-Methylcyclopentyl methacrylate Chemical Properties |
Boiling point | 205.2±9.0 °C(Predicted) | density | 0.96±0.1 g/cm3(Predicted) | form | clear liquid | color | Colorless to Light yellow |
| 1-Methylcyclopentyl methacrylate Usage And Synthesis |
Chemical Properties | Colorless to Light yellow clear liquid | Uses | 1-Methylcyclopentyl methacrylate is used as Photoresist monomer. | Preparation | The preparation of 1-Methylcyclopentyl methacrylate is as follows:Add 1-methylcyclopentanol (730g, 7.29mol), dichloromethane (5100g), triethylamine (1819g, 17.98mol), 4-dimethylaminopyridine (8.9g, 0.0728mol) to the 10L four-necked flask Stirring and cooling with phenothiazine (7.3g) were started, and methacryloyl chloride (1143g, 10.93mol) was added dropwise at a temperature of 0 to 5℃., and the temperature was kept for 2h after the dropwise addition. (raw material≦2.0%).Water (2000g) was added to quench, and the temperature was controlled not to exceed 20℃. The organic phase was washed twice with 5% hydrochloric acid (2000g*2), twice with 5% aqueous sodium hydroxide solution (2000g*2), and twice with water (2000g*2), the organic phase was dried by adding anhydrous sodium sulfate, and spun. The solvent was evaporated and concentrated to obtain 1268g of crude product. The crude product was distilled under reduced pressure (negative pressure: 1mmHg column, external temperature: 60-70℃., main fraction: 35-40℃.) to obtain 921g of product. | Application | 1-Methylcyclopentyl methacrylate can be applied in analog semiconductor, light-emitting diode LED, solar photovoltaic and other fields. | Solubility in organics | Very soluble in N,N-Dimethylformamide. Soluble in methanol. Sparingly
soluble inglacial acetic acid. Very slightly soluble inchloroform. Practically insoluble in water. |
| 1-Methylcyclopentyl methacrylate Preparation Products And Raw materials |
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