ChemicalBook Product Catalog Chemical Reagents Organic reagents Imide N-(Chloromethyl)phthalimide

N-(Chloromethyl)phthalimide

N-(Chloromethyl)phthalimide Basic information
Product Name:N-(Chloromethyl)phthalimide
Synonyms:AKOS BBS-00000871;2-(CHLOROMETHYL)-1H-ISOINDOLE-1,3(2H)-DIONE;TIMTEC-BB SBB000346;N-(CHLOROMETHYL)PHTHALIMIDE;1H-Isoindole-1,3(2H)-dione, 2-(chloromethyl)-;2-(chloromethyl)-1h-isoindole-3(2h)-dione;Chloromethylphthalimide;N-Chloromethyltrimellitimide
CAS:17564-64-6
MF:C9H6ClNO2
MW:195.6
EINECS:241-541-4
Product Categories:API Intermediate;Carbonyl Compounds;Cyclic Imides;Organic Building Blocks;N-Substituted Maleimides, Succinimides & Phthalimides;N-Substituted Phthalimides;UV Detection (HPLC Labeling Reagents);Analytical Chemistry;Carboxyl Group Labeling Reagents for HPLC;HPLC Labeling Reagents
Mol File:17564-64-6.mol
N-(Chloromethyl)phthalimide Structure
N-(Chloromethyl)phthalimide Chemical Properties
Melting point 131-135 °C (lit.)
Boiling point 305.2±25.0 °C(Predicted)
density 1.3228 (rough estimate)
refractive index 1.5790 (estimate)
storage temp. 2-8°C
solubility chloroform: soluble50mg/mL
form powder to crystal
pka-2.63±0.20(Predicted)
color White to Almost white
Water Solubility slightly soluble
BRN 140942
CAS DataBase Reference17564-64-6(CAS DataBase Reference)
NIST Chemistry ReferenceN-(chloromethyl)phthalimide(17564-64-6)
EPA Substance Registry System1H-Isoindole-1,3(2H)-dione, 2-(chloromethyl)- (17564-64-6)
Safety Information
Hazard Codes Xi,Xn
Risk Statements 36/37/38-52/53-43-22
Safety Statements 26-36-37/39-61-45
RIDADR UN 2811 6.1 / PGIII
WGK Germany 3
F 9-21
TSCA Yes
HS Code 29251995
MSDS Information
ProviderLanguage
N-(Chloromethyl)phthalimide English
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ACROS English
ALFA English
N-(Chloromethyl)phthalimide Usage And Synthesis
Chemical Propertieswhite crystalline powder
UsesIt is used as an agrochemical and medicine intermediates and is used in organic synthesis. Microporous membranes prepared from chemically modified polysulfone, which is a derivative of this compound have better streaming potential.
Purification MethodsPurify the imide by recrystallisation from EtOAc or CCl4 or via the 1:1 complex with pyridine [Sakellarios J Am Chem Soc 70 2822 1948, B.hme et al. Chem Ber 92 1258 1959]. [Beilstein 21/10 V 372.]
N-(Chloromethyl)phthalimide Preparation Products And Raw materials
Raw materialsToluene-->Phthalimide
Preparation ProductsBIS(DIETHYLAMINO)CHLOROPHOSPHINE-->2-[(3-CHLOROPHENOXY)METHYL]-1H-ISOINDOLE-1,3(2H)-DIONE
N-CHLOROMETHYL-4-NITROPHTHALIMIDE Chloromethyl methyl ether N-Hydroxyphthalimide Bismaleimide 4-Nitrophthalimide 2-methyl-benzenemethanaminhydrochloride Phthalhydrazide N-METHYL-O-TOLUAMIDE DIALIFOS DIMETHYLFORMAMIDE HYDROGEN CHLORIDE COMPLEX 1,3-DIOXO-1,3-DIHYDRO-ISOINDOLE-2-CARBONYL CHLORIDE N-METHYL-N-(2-METHYLBENZYL)AMINE 3-Nitrophthalimide 2-METHYLISOINDOLIN-1-ONE N-Methylphthalimide Potassium phthalimide ISOINDOLINE 4-Aminophthalimide
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