4,4''-Dimethoxyazoxybenzene

4,4''-Dimethoxyazoxybenzene Basic information
Product Name:4,4''-Dimethoxyazoxybenzene
Synonyms:1,2-Bis(4-methoxyphenyl)diazene;4,4'-Azodianisole;Bis(4-methoxyphenyl)diazene;Diazene, 1,2-bis(4-methoxyphenyl)-;Apixaban Impurity 123;Apixaban Impurity 221
CAS:501-58-6
MF:C14H14N2O2
MW:242.27
EINECS:
Product Categories:
Mol File:501-58-6.mol
4,4''-Dimethoxyazoxybenzene Structure
4,4''-Dimethoxyazoxybenzene Chemical Properties
Boiling point 385.1°C (rough estimate)
density 1.1338 (rough estimate)
refractive index 1.6419 (estimate)
Safety Information
MSDS Information
4,4''-Dimethoxyazoxybenzene Usage And Synthesis
Purification MethodsChromatograph it on basic alumina and elute with *benzene. Then crystallise the residue from 2:2:1 (v/v) methanol/ethanol/*benzene or Me2CO. [Beilstein 16 H 112, 16 I 237, 16 II 43, 16 III 93, 16 IV 172.]
4,4''-Dimethoxyazoxybenzene Preparation Products And Raw materials
Raw materials4-METHOXYAZOBENZENE-->p-Anisidine
Preparation ProductsDiazene, 1,2-diphenyl-, stereoisomer-->N-Benzylideneamine-->6-Methoxyquinoline

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