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| | 4,6-Dichloro-5-nitropyrimidine Basic information |
| | 4,6-Dichloro-5-nitropyrimidine Chemical Properties |
| | 4,6-Dichloro-5-nitropyrimidine Usage And Synthesis |
| Chemical Properties | Yellow Crystalline Solid | | Uses | 4,6-Dichloro-5-nitropyrimidine (cas# 4316-93-2) is a compound useful in organic synthesis. | | Purification Methods | If too impure, then dissolve it in Et2O, wash it with H2O, dry it over MgSO4, evaporate it to dryness and recrystallise it from pet ether (b 85-105o) to give a light tan solid. It is soluble in ca 8 parts of MeOH [Boon et al. J Chem Soc 96 1951, Montgomery et al. in Synthetic Procedures in Nucleic Acid Chemistry Zorbach & Tipson eds, Wiley & Sons, NY, p76 1968]. [Beilstein 23 III/IV 899.] |
| | 4,6-Dichloro-5-nitropyrimidine Preparation Products And Raw materials |
| Raw materials | Nitric acid-->Phosphorus oxychloride-->Trifluoroacetic acid-->N,N-Diisopropylethylamine-->4,6-Dihydroxypyrimidine-->4,6-DIHYDROXY-5-NITROPYRIMIDINE-->5-Nitropyrimidine-4,6(1H,5H)-dione-->4-Pyrimidinamine, 6-chloro-N-methyl-5-nitro-N-phenyl--->6-Chloro-5-nitro-4(1H)-pyrimidinone-->N,N-Dimethylaniline | | Preparation Products | Adenine-->6-Methylpurine-->4,6-Pyrimidinediamine,N4,N6-dimethyl-5-nitro--->N-benzyl-6-chloro-5-nitro-4-pyrimidinamine-->IFLAB-BB F2124-0140-->IFLAB-BB F2124-0129-->IFLAB-BB F2124-0130 |
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