Borane-2-picoline complex

Borane-2-picoline complex Basic information
Product Name:Borane-2-picoline complex
Synonyms:2-Methylpyridine borane complex;2-Methylpyridine - borane (1:1);Borane - 2-Picoline Complex 2-Picoline Borane 2-Methylpyridine Borane;orane-2-picoline coMplex;BORANE - 2-PICOLINE COMPLEX;2-methylpyridine borane;2-picoline borane;borane - 2-methylpyridine complex
CAS:3999-38-0
MF:C6H10BN
MW:106.96
EINECS:609-767-1
Product Categories:B (Classes of Boron Compounds);Boranes;Reduction;Synthetic Organic Chemistry;3999-38-0
Mol File:3999-38-0.mol
Borane-2-picoline complex Structure
Borane-2-picoline complex Chemical Properties
Melting point 48 °C
density 1.297 g/mL at 25 °C
Fp 100°(212°F)
storage temp. 2-8°C
solubility Dichloromethane (Sparingly), Ethyl Acetate (Slightly)
form Solid
color White
Water Solubility Slightly sol. in water, cyclohexane, very sol. in methanol, THF, diglyme, and benzene
Sensitive Moisture Sensitive
InChIKeyZMASBEFBIXMNCP-UHFFFAOYSA-N
Safety Information
Hazard Codes F,Xn,Xi
Risk Statements 14/15-40-36/37/38-26
Safety Statements 36/37-43-26-36/37/38-14/15
RIDADR UN 3130 6.1(4.3) / PGII
WGK Germany 3
HazardClass 4.3
PackingGroup II
HS Code 29333990
MSDS Information
Borane-2-picoline complex Usage And Synthesis
UsesEnvironmentally benign reducing agent. Reactant for: Reductive amination. N-Benzyl-protection of amino acid derivatives by reductive alkylation. Reductive alkoxyamination.
UsesUsed as reactant for N-Benzyl-protection of amino acid derivatives by reductive alkylation, reductive alkoxyamination, as reducing agent for the labeling of oligosaccharides by reductive amination, synthesis of alkoxyamine derivatives, via reduction of oxime ethers, reductive amination reactions of C1-C10 aldehyde 2,4-dinitrophenylhydrazones, synthesis of various trifluoromethylated amino compounds and an alternative reagent for reductive aminations.
General Description2-Methylpyridine borane complex is a nontoxic alternate to the reducing agent sodium cyanoborohydride.
Borane-2-picoline complex Preparation Products And Raw materials
1-BENZYL-2-ISOPROPYL-4,6-DIPHENYLPYRIDINIUM TETRAFLUOROBORATE Boron RARECHEM AQ NN 0231 1-BENZYL-2-METHYL-4,6-DIPHENYLPYRIDINIUM TETRAFLUOROBORATE 2,6-DIETHYL-4-PHENYL-1-[3-(TRIFLUOROMETHYL)BENZYL]PYRIDINIUM TETRAFLUOROBORATE 2-Chloro-5-chloromethylpyridine 2-Picoline Borane-2-picoline complex 4-Methylpyridine Methoxydiethylborane Azamethiphos 2-METHYL-4,6-DIPHENYL-1-PROPYLPYRIDINIUM TETRAFLUOROBORATE 2,6-Lutidine 2,4,6-Collidine INTERMEDIATES 1-FLUORO-2,4,6-TRIMETHYLPYRIDINIUM TETRAFLUOROBORATE Borane-tetrahydrofuran complex Boron nitride

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