Dibenz[b,f]azepine-5-carbonyl chloride

Dibenz[b,f]azepine-5-carbonyl chloride Basic information
Product Name:Dibenz[b,f]azepine-5-carbonyl chloride
Synonyms:CHLOROCARBONYL LIMINOSTILBEN;DIBENZ [B,F]AZEPINE-5-CARBONYL CHLORIDE;IMINOSTILBENE-5-CARBONYL CHLORIDE;IMINOSTILBENE CARBONYL CHLORIDE;5-chlorocarbonyl iminostilbene;5H-DIBENZ[B,F]AZEPINE-5-CARBONYL CHLORIDE;5-(Chlorocarbonyl)-5H-dibenzo[b,f]azepine;N-Chlorocarbonyliminostilbene
CAS:33948-22-0
MF:C15H10ClNO
MW:255.7
EINECS:412-100-5
Product Categories:Building Blocks;Chemical Synthesis;Heterocyclic Building Blocks;N-Containing;Others;Heterocyclic Building Blocks;Aromatics;Heterocycles;Intermediates;Intermediates & Fine Chemicals;Pharmaceuticals
Mol File:33948-22-0.mol
Dibenz[b,f]azepine-5-carbonyl chloride Structure
Dibenz[b,f]azepine-5-carbonyl chloride Chemical Properties
Melting point 149-153 °C (lit.)
Boiling point 413.7±38.0 °C(Predicted)
density 1.316±0.06 g/cm3(Predicted)
solubility soluble in Chloroform, Dichloromethane, Ethyl Acetate
pka-3.69±0.20(Predicted)
form Oil
color Brown
CAS DataBase Reference33948-22-0(CAS DataBase Reference)
Safety Information
Hazard Codes C
Risk Statements 34
Safety Statements 26-36/37/39-45
RIDADR UN 3261 8/PG 2
WGK Germany 3
MSDS Information
ProviderLanguage
SigmaAldrich English
Dibenz[b,f]azepine-5-carbonyl chloride Usage And Synthesis
Chemical PropertiesPink Solid
UsesDibenz [b,f]azepine-5-carbonyl chloride may be used in the preparation of trans-10,11-dibromo-10,11-dihydro-5H-dibenz[b,f]azepine-5-carbonyl chloride via bromination using bromine. It may also be used to prepare urea derivatives, which are potent P2X4 receptor (purinergic receptor) antagonists.
UsesAn intermediate in the preparation of Carbamazepine.
General DescriptionDibenz [b,f]azepine-5-carbonyl chloride or 5H-dibenz [b,f]azepine-5-carbonyl chloride is a tricyclic heterocyclic compound that can be synthesized from 5H-dibenz[ b,f]azepine.
Dibenz[b,f]azepine-5-carbonyl chloride Preparation Products And Raw materials
Raw materialsIron-->Sodium Methoxide-->2-Nitrotoluene-->Iminostilbene-->2,2'-ETHYLENEDIANILINE
Methylene Chloride 4-Nitrobenzoyl chloride 2-Fluorobenzoyl chloride PYRAZOPHOS Sodium chloride N-Acetylsulfanilyl chloride CARBONYL SULFIDE Choline chloride Methanesulfonyl chloride Ammonium chloride Oxalyl chloride 4-Chlorobenzoyl chloride Iminostilbene Benzoyl chloride Potassium chloride Thionyl chloride 2-​[[(2-​ethylphenyl)​(2-​hydroxyethyl)​amino]​methyl]​-​3,​3-​difluoro-Propanenitrile p-Toluoyl chloride

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