N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine

N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Basic information
Product Name:N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine
Synonyms:N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine;1,3-Benzenediamine, N3-[1,1'-biphenyl]-4-yl-N1,N1-diphenyl-
CAS:1800322-10-4
MF:C30H24N2
MW:412.52
EINECS:
Product Categories:
Mol File:1800322-10-4.mol
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Structure
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Chemical Properties
Safety Information
MSDS Information
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Usage And Synthesis
Synthesis2.jpg
Diphenylamine (37.0 g, 218.64 mmol) was added to a round bottom flask and dissolved in toluene (1100 mL), and 1-bromo-3-chlorobenzene 41.86 g, 218.64 mmol), Pd2(dba)3 (6.01 g, 6.56 mmol), P(t-Bu)3 (2.65 g, 13.12 mmol), NaOt-Bu (63.03 g, 655.9 mmol) were added in the order and stirred at 100 ° C. After the reaction was completed, the reaction mixture was extracted with ether and water. The organic layer was dried over MgSO4 and concentrated. The resultingcompound wasseparated bysilicagelcolumn chromatography andrecrystallized to obtain47.6 g ofthe product. (yield: 78%)
N3-[1,1'-Biphenyl]-4-yl-N1,N1-diphenyl-1,3-benzenediamine Preparation Products And Raw materials

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