ChemicalBook Product Catalog Organic Chemistry Heterocyclic Compounds 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Basic information
Product Name:2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
Synonyms:2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine;1,3,5-Triazine, 2-(4-broMophenyl)-4,6-diphenyl-;PTZ-Br;)-4,6-diphenyL;1,3,5-Triazine, 2-(4-bromopheny)-4,6-dipheny-;2-(4-bromophenyl)-4;23449-08-3 1,3,5-Triazine, 2-(4-bromophenyl)-4,6-diphenyl-
CAS:23449-08-3
MF:C21H14BrN3
MW:388.26
EINECS:
Product Categories:1,3,5-triazine;oled intermediate;23449-08-3
Mol File:23449-08-3.mol
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Structure
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Chemical Properties
Melting point 200.0 to 204.0 °C
Boiling point 573.9±52.0 °C(Predicted)
density 1.381
storage temp. Sealed in dry,Room Temperature
form powder to crystal
pka0.45±0.10(Predicted)
color White to Almost white
InChIKeyAYHGAQGOMUQMTR-UHFFFAOYSA-N
Safety Information
HS Code 29336990
MSDS Information
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Usage And Synthesis
Chemical Propertieswhite solid powder
SynthesisThe compound, 2-chloro-4,6-diphenyl-1,3,5-triazine (50 g, 187 mmol) was dissolved in THF (1 L) under a nitrogen environment, (4-bromophenyl)boronic acid (45 g, 224.12 mmol, Aldrich Corporation), and tetrakis(triphenylphosphine)palladium (2.1 g, 1.87 mmol) were added thereto, and the mixture was stirred. Potassium carbonate saturated in water (64 g, 467 mmol) was added thereto, and the obtained mixture was heated and refluxed at 80° C. for 12 hours. When the reaction was complete, water was added to the reaction solution, and the mixture was extracted with dichloromethane (DCM) and then, filtered after removing moisture with anhydrous MgSO4 and concentrated under a reduced pressure. This obtained residue was separated and purified through flash column chromatography to obtain 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine (70 g and 96%).
2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Preparation Products And Raw materials
Raw materials2-chloro-4,6-diphenyl-1,3,5-triazine-->4-Bromophenylboronic acid
2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole 2-chloro-4,6-di(naphthalen-2-yl)-1,3,5-triazine 2-(3'-BroMo-biphenyl-3-yl)-4,6-diphenyl-[1,3,5]triazine 2-(3-Bromophenyl)-4,6-diphenyl-1,3,5-triazine 2-chloro-4-(biphenyl-4-yl)-6-phenyl-1,3,5-triazine 2-(2-bromophenyl)-4,6-diphenyl-1,3,5-triazine (1α,2α,3aα,4α,7α,7aα)- 2-ethenyl-2,3,3a,4,7,7a-hexahydro-4,7-Methano-1H-indene-1-methanol 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine 1,3,5-Triazine, 2-(4-bromo-1-naphthalenyl)-4,6-diphenyl- Tribromobenzene 2,4-Dichloro-6-phenyl-1,3,5-triazine Benzyl bromide 2-(3'-Chloro[1,1'-biphenyl]-3-yl)-4,6-diphenyl-1,3,5-triazine 2-(3-broMo-5-chlorophenyl)-4,6-diphenyl-1,3,5-triazine 2-(4-Biphenylyl)-4,6-dichloro-1,3,5-triazine 2-(2-BroMophenyl)-9H-phenylcarbazole TPP 2-(3,5-Dibromophenyl)-4,6-diphenyl-1,3,5-triazine
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