2-Amino-5-iodobenzoic acid

2-Amino-5-iodobenzoic acid Basic information

Product Name:	2-Amino-5-iodobenzoic acid
Synonyms:	TIMTEC-BB SBB001006;2-amino-5-iodo-benzoicaci;2-AMINO-5-IODOBENZOIC ACID (5-IODOANTHRANILIC ACID);2-AMino-5-iodobenzoic acid, 98% 25GR;2-Amino-5-iodobenzoic acid;5-iodo-anthranilicaci;5-Iodoanthranillic acid;5-iodoanthranil acid
CAS:	5326-47-6
MF:	C7H6INO2
MW:	263.03
EINECS:	226-205-7
Product Categories:	Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts;Carboxylic Acids;Phenyls & Phenyl-Het;Benzoic acid;Organic acids;API intermediates;Acids & Esters;Anilines, Amides & Amines;Iodine Compounds;Carboxylic Acids;Phenyls & Phenyl-Het
Mol File:	5326-47-6.mol

2-Amino-5-iodobenzoic acid Chemical Properties

Melting point	219-221 °C (dec.) (lit.)
Boiling point	383.2±37.0 °C(Predicted)
density	1.8886 (estimate)
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
solubility	DMSO (Slightly), Methanol (Slightly)
pka	4.59±0.10(Predicted)
form	Crystalline Powder
color	Beige or gray to purple
Water Solubility	Soluble in alcohol. Insoluble in water.
Sensitive	Light Sensitive
BRN	639029
InChIKey	GOLGILSVWFKZRQ-UHFFFAOYSA-N
CAS DataBase Reference	5326-47-6(CAS DataBase Reference)
EPA Substance Registry System	5-Iodoanthranilic acid (5326-47-6)

Safety Information

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-36-37/39
WGK Germany	3
RTECS	DG2802000
Hazard Note	Irritant
TSCA	T
HazardClass	IRRITANT, LIGHT SENSITIVE
HS Code	29224995

MSDS Information

Provider	Language
2-Amino-5-iodobenzoic acid	English
SigmaAldrich	English
ACROS	English
ALFA	English

2-Amino-5-iodobenzoic acid Usage And Synthesis

Synthesis	To the mixture of 2.89 g (18.2 mmol) sodium 2- aminobenzoate, 40 mL acetic acid and 2.31 g (9.1 mmol) molecular iodine, 5 mL (44.1 mmol, 30 wt %) aqueous hydrogen peroxide was added drop wise. The S3 reaction mixture was stirred at 50 °C for 3 h and poured into 400 mL water. The formed crystals were filtered and recrystallized from benzene to give 2-azido-5- iodobenzoic acid . IR (suspension in nujol, cm−1 ): 3500, 3387, 1670, 1612, 1580, 1541, 1419, 1377, 1319, 1290, 1163, 1125, 813, 688, 619.
Chemical Properties	white to light yellow crystal powder
Uses	2-Amino-5-iodobenzoic acid is used in wide range of medicals industrial applications as well as in human and animal nutrition products such as pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals.

2-Amino-5-iodobenzoic acid Preparation Products And Raw materials

Raw materials	Acetic acid-->Potassium hydroxide-->Sodium bisulfite-->Iodine-->Anthranilic acid-->Iodine monochloride-->Iodine chloride solution (Wijs' chloride)
Preparation Products	2,3,5-Triiodobenzoic acid-->5-Iodoisobenzofuran-1,3-dione-->2-Amino-6-iodoquinazolin-4(1H)-one-->6-Iodo-2-phenyl-4H-benzo[d][1,3]oxazin-4-one

3,5-DIIODO-2-[[[[3-(PHENOXYMETHYL)BENZOYL]AMINO]THIOXOMETHYL]AMINO]-BENZOIC ACID 2-[[[[(2-CHLOROPHENOXY)ACETYL]AMINO]THIOXOMETHYL]AMINO]-5-IODO-BENZOIC ACID Ethyl 2-(Chlorosulfonyl)acetate Ascoric Acid METHYL 2-AMINO-3,5-DIIODOBENZOATE Methyl 2-amino-5-iodobenzoate ALTRENOGEST 3,5-DIIODO-2-[[[(2-METHOXYBENZOYL)AMINO]THIOXOMETHYL]AMINO]-BENZOIC ACID 2-[[[(4-CHLORO-1-OXOBUTYL)AMINO]THIOXOMETHYL]AMINO]-3,5-DIIODO-BENZOIC ACID BOC-2-AMINO-5-IODOBENZOIC ACID 2-[[[(3-ETHOXYBENZOYL)AMINO]THIOXOMETHYL]AMINO]-3,5-DIIODO-BENZOIC ACID 2-[[[(2-CHLORO-4-NITROBENZOYL)AMINO]THIOXOMETHYL]AMINO]-5-IODO-BENZOIC ACID 2-[[[(2-BROMO-5-NITROBENZOYL)AMINO]THIOXOMETHYL]AMINO]-5-IODO-BENZOIC ACID Methyl 4-amino-3-iodobenzoate 3,5-DIIODO-2-[[[(3-METHYL-4-NITROBENZOYL)AMINO]THIOXOMETHYL]AMINO]-BENZOIC ACID AMINO ACIDS FMOC-2-AMINO-5-IODOBENZOIC ACID 2-[[[[[5-(2,5-DICHLOROPHENYL)-2-FURANYL]CARBONYL]AMINO]THIOXOMETHYL]AMINO]-3,5-DIIODO-BENZOIC ACID

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