BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE

BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE Basic information
Product Name:BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE
Synonyms:BIS(2,2,2-TRICHLOROETHYL) AZODI-CARBOXYL ATE, 97+%;AZODICARBOXYLIC ACID BIS(2,2,2-TRICHLOROETHYL) ESTER;BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE;Bis(2,2,2-trichloroethyl) azodicarboxyle;BEAZ Bis(2,2,2-trichloroethyl) azodicarboxylate;1,2-Diazenedicarboxylic acid, 1,2-bis(2,2,2-trichloroethyl) ester
CAS:38857-88-4
MF:C6H4Cl6N2O4
MW:380.83
EINECS:
Product Categories:
Mol File:38857-88-4.mol
BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE Structure
BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE Chemical Properties
Melting point 109-111 °C (lit.)
Boiling point 380.7±42.0 °C(Predicted)
density 1.78±0.1 g/cm3(Predicted)
storage temp. 2-8°C
BRN 2141527
CAS DataBase Reference38857-88-4
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 3
MSDS Information
ProviderLanguage
SigmaAldrich English
BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE Usage And Synthesis
Chemical PropertiesYellow powder or crystals
UsesBis(2,2,2-trichloroethyl) azodicarboxylate has been used:
  • in the asymmetric synthesis of substituted cycloalkyl[b]indoles
  • as amination reagent during the aza-ene reaction of different alkenes to yield the corresponding allyl amines
  • in para-directed amination of C2-alkyl substituted anisole
  • in the synthesis of acid- and base-sensitive azo compounds and in Diels-Alder cycloadditions
General DescriptionThermal inverse-type hetero-Diels-Alder reaction of O-silyl-protected lactal and bis(2,2,2-trichloroethyl) azodicarboxylate has been reported.
BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE Preparation Products And Raw materials
BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE 1,1,1-Trichloroethane Chloroform Diethyl azodicarboxylate Trichloroethanol AZODICARBOXYLIC ACID DIMETHYL ESTER 4-METHOXYBENZENESULFONAMIDE AMMONIUM CARBAMATE

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