P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE

P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE Basic information
Product Name:P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE
Synonyms:4-TOLUENESULFINIC ACID NA 4H2O;4-TOLUENESULFINIC ACID, SODIUM SALT, TETRAHYDRATE;P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE;SODIUM P-TOLUENESULFINATE TETRAHYDRATE;SODIUM 4-TOLUENESULFINATE TETRAHYDRATE;SodiuM p-Toluenesulfinate ;Sodium p-Toluenesulfinate Tetrahydrate;Sodium P-Toluenesulfinate Tetrahydrate, SPTS, P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE
CAS:868858-48-4
MF:C7H15NaO6S
MW:250.25
EINECS:212-538-5
Product Categories:
Mol File:Mol File
P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE Structure
P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE Chemical Properties
storage temp. Inert atmosphere,Room Temperature
Water Solubility Soluble in water
form powder to crystal
color White to Light yellow
Merck 14,9532
CAS DataBase Reference868858-48-4
Safety Information
RTECS XT4725000
HS Code 2904.10.3700
MSDS Information
P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE Usage And Synthesis
UsesSodium p-toluenesulfinate Hydrate is used in organic chemical reactions as an alkylating agent, non-oxidizing catalyst, intermediate for the synthesis of biologically active compounds. of grades are available including Mil Spec (military grade), ACS, Reagent and Technical Grade, Food, Agricultural and Pharmaceutical Grade, Optical Grade, USP and EP/BP (European Pharmacopoeia/British Pharmacopoeia).
Synthesis2.jpg
The aryl sulfonyl chloride (10.0 mmol, 1.0 equiv) was dissolved in 30 mL water. Sodium sulfite (16.0 mmol, 1.6 equiv) and sodium bicarbonate (16.0 mmol, 1.6 equiv) were added, and the reaction mixture was refluxed for 3 h. The water was evaporated, and ethanol was added to the residue. The suspension was heated for 10 min, cooled, and filtered through a 20 μm polyethylene frit. This was repeated twice with the residue from the filtration. The ethanol fractions were combined, and the solvent was evaporated under vacuum, The sodium arylsulfinates were isolated as white powders.
P-TOLUENESULFINIC ACID SODIUM SALT TETRAHYDRATE Preparation Products And Raw materials
p-Toluenesulfonic acid monohydrate 4'-Methylacetophenone P-TOLUENESULFINIC ACID

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