DIMETHYL PHOSPHOROCHLORIDATE

DIMETHYL PHOSPHOROCHLORIDATE Basic information

Product Name:	DIMETHYL PHOSPHOROCHLORIDATE
Synonyms:	DIMETHYL CHLOROPHOSPHATE;DIMETHYL PHOSPHOROCHLORIDATE;Chlorodimethoxyphosphine oxide;Chlorodimethylphosphate;Dimethoxyphosphinic chloride;Dimethyl chloridophosphate;Dimethyl chlorophosphonate;Dimethyl phosphorchloridate
CAS:	813-77-4
MF:	C2H6ClO3P
MW:	144.49
EINECS:
Product Categories:	Aliphatics;Phospholipids - 13C & 2H;Phosphorylating and Phosphitylating Agents
Mol File:	813-77-4.mol

DIMETHYL PHOSPHOROCHLORIDATE Chemical Properties

Boiling point	80 °C/25 mmHg (lit.)
density	1.34 g/mL at 25 °C (lit.)
refractive index	n20/D 1.413(lit.)
Fp	>230 °F
solubility	Acetonitrile (Slightly), Chloroform (Slightly)
form	clear liquid
color	Colorless to Almost colorless
Stability:	Hygroscopic, Moisture Sensitive
CAS DataBase Reference	813-77-4

Safety Information

Hazard Codes	T+
Risk Statements	26/27/28-34
Safety Statements	26-36/37/39-45-7/9
RIDADR	UN 2927 6.1/PG 1
WGK Germany	3
HS Code	29199000

MSDS Information

Provider	Language
SigmaAldrich	English

DIMETHYL PHOSPHOROCHLORIDATE Usage And Synthesis

Chemical Properties	Clear Liquid
Uses	A phosphorylating agent
Uses	Dimethyl chlorophosphate may be used for the preparation of (E)-3-cyanophosphoenolpyruvate, by reaction with the potassium enolate of ethyl cyanopyruvate. It may be used for the synthesis of mono- and diphosphate esters of 2-arachidonyl glyceryl ether.
Synthesis Reference(s)	Canadian Journal of Chemistry, 34, p. 1819, 1956 DOI: 10.1139/v56-235 Synthetic Communications, 23, p. 1771, 1993 DOI: 10.1080/00397919308011275

DIMETHYL PHOSPHOROCHLORIDATE Preparation Products And Raw materials

Raw materials	Ethanol-->Hydrogen-->Dimethyl phosphite-->DIMETHYLCHLOROPHOSPHITE-->Methanol-->Carbon tetrachloride-->Sodium Methoxide-->Trimethyl phosphite-->Tin tetrachloride-->Trichloroacetonitrile
Preparation Products	N-methyl-N-methylsulfonyl-methanesulfonamide-->DIMETHYL-P-NITROPHENYLPHOSPHATE-->FENCHLORPHOS-OXON-->Diphosphoric acid P1,P1-diethyl-P2,P2-dimethyl ester

Diphenyl chlorophosphate DIMETHYL PHOSPHOROCHLORIDATE (4R,5R)-2-CHLORO-4,5-DIMETHYL-1,3,2-DIOXAPHOSPHOLANE 2-OXIDE 2-Chloro-1,3,2-dioxaphospholane-2-oxide BIS[2-(P-NITROPHENYL)ETHYL] PHOSPHOROCHLORIDATE Diethyl chlorophosphate Bis(2,4-dichlorophenyl) chlorophosphate BIS(2-CHLOROPHENYL) PHOSPHOROCHLORIDATE BIS(2,2,2-TRICHLOROETHYL) PHOSPHOROCHLORIDATE CHLOROPHOSPHORIC ACID BIS(2,6-DIMETHYLPHENYL) ESTER Dipropyl chlorophosphate 4-TERT-BUTYL-2-CHLOROPHENYL-2,2,2-TRIBROMOETHYL PHOSPHOROCHLORIDATE Diisopropyl chlorophosphate BIS(2,2,2-TRICHLORO-1,1-DIMETHYLETHYL) PHOSPHOROCHLORIDATE BIS(4-CHLOROPHENYL) PHOSPHOROCHLORIDATE 1,2-PHENYLENE PHOSPHOROCHLORIDATE BIS(2-NITROBENZYL) PHOSPHOROCHLORIDATE (2-CHLOROPHENYL)(2,2,2-TRICHLOROETHYL) CHLOROPHOSPHATE

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