3-Chlorobenzaldehyde

3-Chlorobenzaldehyde Basic information

Product Name:	3-Chlorobenzaldehyde
Synonyms:	AKOS BBS-00003158;Benzaldehyde, 3-chloro-;3-Chlorbenzaldehyd;3-Chlorobenzaldehyde98%;3-Chlorobenzaldehyde 98%;Chlorobenzaldehyde-3;3-Chlorobenzaldehyde,97%;3-CHLOROBENZALDEHYDE GRADE A
CAS:	587-04-2
MF:	C7H5ClO
MW:	140.57
EINECS:	209-596-9
Product Categories:	Aldehydes;C7;Carbonyl Compounds;Aromatic Aldehydes & Derivatives (substituted);FINE Chemical & INTERMEDIATES
Mol File:	587-04-2.mol

3-Chlorobenzaldehyde Chemical Properties

Melting point	9-12 °C (lit.)
Boiling point	213-214 °C (lit.)
density	1.241 g/mL at 25 °C (lit.)
refractive index	n20/D 1.563(lit.)
Fp	191 °F
storage temp.	Keep in dark place,Inert atmosphere,2-8°C
form	Liquid
Specific Gravity	1.235
color	Clear colorless to light yellow
Water Solubility	insoluble
Sensitive	Air Sensitive
BRN	507098
CAS DataBase Reference	587-04-2(CAS DataBase Reference)
NIST Chemistry Reference	Benzaldehyde, 3-chloro-(587-04-2)
EPA Substance Registry System	Benzaldehyde, 3-chloro- (587-04-2)

Safety Information

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-36-37/39
RIDADR	2810
WGK Germany	2
F	1-9
Hazard Note	Irritant
TSCA	Yes
HS Code	29130000

MSDS Information

Provider	Language
3-Chlorobenzaldehyde	English
SigmaAldrich	English
ACROS	English
ALFA	English

3-Chlorobenzaldehyde Usage And Synthesis

Chemical Properties	clear colourless to light yellow liquid
Uses	3-Chlorobenzaldehyde, is used as a medicine, dye intermediates and speciality chemicals. It is mainly used to produce medicine material and intermediate, chloral alcoholate and intermediate of acid mordant azurine-6B on dyestuff.
Synthesis Reference(s)	The Journal of Organic Chemistry, 48, p. 4053, 1983 DOI: 10.1021/jo00170a036 Tetrahedron Letters, 22, p. 11, 1981 DOI: 10.1016/0040-4039(81)80027-5
Purification Methods	Purify it by low temperature crystallisation from pet ether (b 40-60o) and distillation. [Beilstein 7 H 234, 7 IV 566.]

3-Chlorobenzaldehyde Preparation Products And Raw materials

Raw materials

Copper(I) chloride-->Stannous chloride dihydrate-->3-Nitrobenzaldehyde-->1-Chloro-3-iodobenzene-->Methanediol, (3-chlorophenyl)-, diacetate-->2-(3-Chlorophenyl)-1,3-dithiane-->3-Chlorostyrene

Preparation Products

2-(3-Chlorophenyl)ethylamine-->3-(3-CHLORO-PHENYL)-PROPIONALDEHYDE-->3-Chlorobenzylamine-->5-CHLORO-1H-INDAZOLE-3-CARBOXYLIC ACID-->3-(3-CHLOROPHENYL)PROPIONIC ACID-->3-CHLORO-N-METHYLBENZYLAMINE-->5-Chloro-2-nitrobenzaldehyde-->L-3-Chlorophenylalanine-->2,5-Dichlorobenzaldehyde-->1-Bromo-4-chloro-2-methylbenzene-->3-Cyanobenzaldehyde-->3-CHLORO-THIOBENZAMIDE-->1-(3-Chlorophenyl)-2-hydroxy-1-propanone-->3-CHLOROPHENYLACETONE

2-Bromo-5-chlorobenzaldehyde 3-BROMO-4-CHLOROBENZALDEHYDE 3-chlorobenzaldehyde 1,3-thiazol-2-ylhydrazone 3',4'-DICHLOROACETOPHENONE O-nitro chloro benzaldehyde 2-chlorobenzaldehyde (4-methyl-3-phenyl-1,3-thiazol-2(3H)-ylidene)hydrazone 3',4'-DICHLOROPROPIOPHENONE 3’-Chloroacetophenone m-Phthalaldehyde Methyl 3-chlorobenzoate 2-[2-(4-tert-butylphenoxy)ethoxy]-5-chlorobenzaldehyde (4,6-dipyrrolidin-1-yl-1,3,5-triazin-2-yl)hydrazone 4-chlorobenzaldehyde [4-(3-chloro-4-methylanilino)-6-(4-morpholinyl)-1,3,5-triazin-2-yl]hydrazone 2-(4-CHLOROBENZYLIDENE)HYDRAZINE-1-CARBOTHIOAMIDE 2-Chloro-N-[4-chloro-2-(2-chlorobenzoyl)phenyl]acetamide IMP. A (EP): CHLORPHENAMINE (USP: CHLORPHENIRAMINE) p-Dichlorobenzene 3-chlorobenzaldehyde [4,6-di(1-pyrrolidinyl)-1,3,5-triazin-2-yl]hydrazone 4-chlorobenzaldehyde {[1-ethyl-2-oxo-6-(6-oxo-1,4,5,6-tetrahydro-3-pyridazinyl)-1,2-dihydro-3H-indol-3-ylidene]methyl}hydrazone

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